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Heat treatment method for grain refinement of NiCrMoV steel forging piece

A heat treatment method and grain refinement technology, which is applied in the field of heat treatment of forgings, can solve problems such as the difficulty in judging the internal quality of forgings, the decline in mechanical properties of forgings, and the interference of defect signals, so as to ensure performance, improve the structure state, and improve stability. Effect

Active Publication Date: 2013-09-18
MAGANG (GROUP) HOLDING CO LTD +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Since the structure of the forging is a non-equilibrium structure of coarse grain, the original coarse grain state will be retained due to the inheritance of the structure when the final heat treatment is carried out directly, resulting in a decline in the mechanical properties of the forging, and also causing grass-like waves in the waveform of the forging during ultrasonic flaw detection, which interferes with the defect signal , making it difficult or even impossible to judge the internal quality of forgings

Method used

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  • Heat treatment method for grain refinement of NiCrMoV steel forging piece
  • Heat treatment method for grain refinement of NiCrMoV steel forging piece
  • Heat treatment method for grain refinement of NiCrMoV steel forging piece

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] Example 1, Example 2 and Example 3 Chemical composition of forgings (mass percentage, wt-%)

[0033]

C

Si

Mn

P

S

Cr

Ni

Mo

V

Examples 1, 2

0.34

0.32

0.29

0.005

0.004

1.24

3.26

0.38

0.14

[0034] Example 3

0.37

0.11

0.21

0.007

0.005

1.39

3.23

0.33

0.13

[0035] Example 1:

[0036] Example 1 is a test conducted under laboratory conditions to verify the effectiveness of the technical solution of the present invention. The sample is a metallographic sample of 15×15×15mm. The specific technical scheme is:

[0037] The high temperature normalizing process at 950°C is as follows: heat the metallographic sample at a heating rate of 60°C / hour to 360°C for 0.5 hours, and then heat it to 950°C at a heating rate of 150°C / hour (simulating heating conditions for large forgings) , Heat preservation for 1.5 hours, furnace cooling (simulating air cooling conditions of large forgings) to the sample surface temperature of 200 ℃.

[0038...

Embodiment 2

[0042] The chemical composition of Example 2 is the same as that of Example 1. The diameter of the forging is 450mm. After forging, the following procedures are adopted: 950°C high temperature normalizing step, 900°C high temperature normalizing step, and softening annealing step;

[0043] The specific technical scheme of the heat treatment method is:

[0044] The 950℃ high-temperature normalizing process is: after the forging process, the forgings are directly heated to the furnace, the furnace temperature is 650℃, kept for 5 hours, the furnace is air-cooled to 200℃ on the surface of the forging, and the furnace is loaded. The furnace temperature is kept at 210℃. 5 hours, heating to 370°C at a heating rate of 60°C / hour for 3 hours, then heating the furnace to 950°C with maximum power, holding at 950°C for 5 hours, and air cooling to 200°C of the forging surface;

[0045] 900°C high temperature normalizing process: install the furnace, keep the furnace temperature at 210°C for 5 hour...

Embodiment 3

[0049] Forgings with a diameter of 1m use the following procedures after forging: 950℃ high temperature normalizing procedure, 900℃ high temperature normalizing procedure, and softening annealing procedure;

[0050] The specific technical scheme of the heat treatment method is:

[0051] The 950℃ high-temperature normalizing process is: after the forging process is finished, the forging is directly heated to the furnace, the furnace temperature is 640℃, kept for 10 hours, the furnace is air-cooled to 200℃ on the surface of the forging, and the furnace is loaded, and the furnace temperature is kept at 220℃. For 10 hours, heat to 360°C at a heating rate of 40°C / hour for 6 hours, then heat the furnace to 950°C with maximum power, keep it at 950°C for 10 hours, and air-cool to the surface temperature of the forging to 200°C;

[0052] 900°C high temperature normalizing process: install the furnace, keep the furnace temperature at 220°C for about 10 hours, heat to 360°C at a heating rate of...

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Abstract

The invention discloses a heat treatment method for grain refinement of a NiCrMoV steel forging piece. The working procedures after the forging piece is forged are as follows: a high-temperature normalizing procedure at the temperature of 950 DEG C, a high-temperature normalizing procedure at the temperature of 900 DEG C and a softening annealing procedure; and carrying out preheating treatment on the NiCrMoV steel forging piece after being subjected to forging, so that a structural state is obviously improved; the grain is obviously refined; the autstenitic grain size can be improved to 6-8 grades from autstenitic grain size less than or equal to 2 grades after forging; the performance of the forging piece after being subjected to final heat treatment can be effectively ensured and the stability of the forging piece performance is improved.

Description

Technical field [0001] The invention belongs to a heat treatment method for forgings, in particular to a heat treatment method for grain refinement of steel forgings. Background technique [0002] NiCrMoV steel has high hardenability. After austenitization, forgings with a diameter of 1000mm or larger, air cooling or furnace cooling treatment is used after forging stops, and the core can only get bainite-based structure, and it is close to the surface of the forging. The structure is dominated by needle-shaped lower bainite. [0003] Because the structure of the forging is a coarse-grained non-equilibrium structure, the original coarse-grained state will be retained due to the inheritance of the structure when the final heat treatment is directly performed, which will cause the mechanical properties of the forging to decrease, and the waveform of the forging during ultrasonic inspection will appear grass-like waves, which will interfere with the defect signal. , Which makes it dif...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C21D10/00C21D1/28C21D1/32
Inventor 钟斌江波陈刚赵海孙曼丽
Owner MAGANG (GROUP) HOLDING CO LTD