Stable powdered phytic acid composition and preparation method thereof
A composition and powdered technology, applied in the field of powdered phytic acid compositions, can solve the problems of inedibility and the like, and achieve the effects of improving taste, promoting the effect of flavor improvement, and improving quality improvement.
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Embodiment 1
[0066] Next, the preparation method of the preparation example is demonstrated concretely.
[0067] 【Powder preparation (1-1)】
[0068] Put 140 g of anhydrous sodium acetate powder in a mixer with a diameter of 20 cm and two rotating stirring blades up and down, and add a small amount of 30% phytic acid aqueous solution for about 15 minutes while stirring to make uniform adsorption. The mixture is formed at 40-60°C through the exothermic reaction of adsorption, and the temperature gradually decreases during the continuation of stirring. After cooling, the mixture was lightly pulverized and sieved through a 2×2 mm sieve to obtain a powder formulation (1-1).
[0069] 【Powder preparation (1-2)】
[0070] By the same operation as above-mentioned (1-1), 172g of anhydrous sodium acetate powder is stirred in a blender with a small amount of 50% phytic acid aqueous solution 28g, stirred, adsorbed, cooled, pulverized, and sieved to obtain a powder preparation (1 -2).
[0071] 【Powde...
Embodiment 2
[0086] The following powder formulations were prepared in the same manner as the respective formulations of Example 1, and changes over time at room temperature were observed. The results are shown in the table below.
[0087] 【Table 2】
[0088]
[0089] As shown in Table 2, the formulations described in formulation examples (2-1) to (2-3) showed almost no change in color and odor over time, and long-term stability as a powder formulation was confirmed. In addition, the 1% aqueous solution of their powder is almost colorless and odorless.
Embodiment 3
[0091] Based on the method of Example 1, formulations (A) to (Z) were prepared using the components described in Table 3-1 and Table 3-2.
[0092] 【Table 3-1】
[0093]
[0094] 【Table 3-2】
[0095]
[0096] In addition, each emulsifier used in Table 3-1 and Table 3-2 is as follows.
[0097] Hexaglycerol ricinoleate (manufactured by Riken Vitamin Co., Ltd.; trade name: Poem PR-300)
[0098] Tetraglycerol fatty acid ester (manufactured by Sakamoto Pharmaceutical Co., Ltd.; trade name: SYGrista-CR-310)
[0099] Glycerin monofatty acid ester (manufactured by Riken Vitamin Co., Ltd.; brand name: Poem P-200)
[0100] Decaclycerol deca fatty acid ester (manufactured by Sakamoto Pharmaceutical Co., Ltd.; trade name: SY Grista-DA0-7S)
[0101] Decaclycerol fatty acid ester (manufactured by Sakamoto Pharmaceutical Co., Ltd.; trade name: SY Glista-OE-750)
[0102] Distilled diglycerin fatty acid ester (manufactured by Riken Vitamin Co., Ltd.; trade name: Poem DS-100A)
[0103...
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