Method for assessing settleability and uniformity of lithium ion battery anode slurry

A technology for lithium-ion batteries and cathode materials, which can be used in the analysis of materials, by removing certain components, weighing, instruments, etc., to solve the problems of inconsistent internal resistance, non-uniformity, and large differences in physical properties of the battery cells.

Active Publication Date: 2015-05-13
SHENZHEN DYNANONIC
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Especially in today's period when new energy vehicles attract much attention, lithium-ion batteries are more and more widely used; the preparation method of lithium-ion battery cathode material slurry is to mix the main components, such as lithium iron phosphate, conductive agent, binder Add solvents, solvents, etc. to the mixer in turn. Due to the large differences in physical properties such as specific gravity and specific surface among various materials, even if pre-mixed with a mixer in advance, it is difficult to prepare the lithium-ion battery cathode material slurry evenly, and it is prone to sedimentation and unevenness. Uniformity, resulting in poor consistency of the coated pole piece, resulting in inconsistent internal resistance inside the cell, which in turn affects the performance of the lithium-ion battery, and the performance of a small lithium-ion battery is related to the performance of the product. Life and safety, etc., so strengthening control from the source of lithium-ion battery production is the top priority
[0003] At present, most of the methods for testing the sedimentation and uniformity of the positive electrode material slurry of lithium-ion batteries adopt the visual method or take a certain amount of the positive electrode material slurry of the lithium-ion battery and leave it for a period of time to observe its sedimentation and uniformity. The test results are not accurate. Reliable, and the test takes a long time, so a better method is needed to evaluate the settling and uniformity of the cathode material slurry for lithium-ion batteries

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  • Method for assessing settleability and uniformity of lithium ion battery anode slurry
  • Method for assessing settleability and uniformity of lithium ion battery anode slurry
  • Method for assessing settleability and uniformity of lithium ion battery anode slurry

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Experimental program
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Effect test

Embodiment 1

[0035] The components of lithium iron phosphate slurry, a positive electrode material for lithium ion batteries, are shown in Table 1, and the theoretical solid content is 42.00%.

[0036] Table 1 Lithium Iron Phosphate Slurry Components of Lithium-ion Battery Cathode Material

[0037] Element

Lithium iron phosphate

conductive agent

binder

solvent

Proportion (%)

35.00

3.00

4.00

58.00

[0038] A method for evaluating the sedimentation and uniformity of the positive electrode material lithium iron phosphate slurry for lithium ion batteries, comprising the following steps:

[0039] (1) Take the lithium iron phosphate slurry, which is the positive electrode material of lithium-ion batteries, and stir it evenly. Take 3 samples randomly from different positions in the slurry tank, namely A, B, and C. Mark the samples and perform centrifugation at a speed of 2000rmp , the centrifugation time is 30min;

[0040] (2) Divide...

Embodiment 2

[0052] The components of lithium iron phosphate slurry, a positive electrode material for lithium ion batteries, are shown in Table 3, and the theoretical solid content is 45.00%.

[0053] Table 3 Lithium Iron Phosphate Slurry Components of Lithium-ion Battery Cathode Material

[0054] Element

Lithium iron phosphate

conductive agent

binder

solvent

Proportion (%)

38.00

3.00

4.00

55.00

[0055] A method for evaluating the sedimentation and uniformity of the positive electrode material lithium iron phosphate slurry for lithium ion batteries, comprising the following steps:

[0056] (1) Take the lithium iron phosphate slurry, which is the positive electrode material of lithium-ion batteries, and stir it evenly. Take 3 samples randomly from different positions in the slurry tank, namely A, B, and C. Mark the samples and perform centrifugation at a speed of 3000rmp , the centrifugation time is 10min;

[0057] (2) Divi...

Embodiment 3

[0070] The composition of lithium iron phosphate slurry, a positive electrode material for lithium ion batteries, is shown in Table 5, and its theoretical solid content is 40.00%.

[0071] Table 5 Lithium Iron Phosphate Slurry Components of Lithium-ion Battery Cathode Material

[0072] Element

Lithium iron phosphate

conductive agent

binder

solvent

Proportion (%)

33.00

3.00

4.00

60.00

[0073] A method for evaluating the sedimentation and uniformity of the positive electrode material lithium iron phosphate slurry for lithium ion batteries, comprising the following steps:

[0074] (1) Take the lithium iron phosphate slurry, which is the positive electrode material of lithium-ion batteries, and stir it evenly. Take 3 samples randomly from different positions in the slurry tank, namely A, B, and C. Mark the samples and perform centrifugation at a speed of 1000rmp , the centrifugation time is 30min;

[0075] (2) Divi...

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Abstract

The invention discloses a method for assessing settleability and uniformity of lithium ion battery anode slurry. The method comprises the following steps of taking samples from different positions of lithium ion battery anode slurry, detecting solid contents of upper and lower layers in a centrifuge tube by a centrifugation method and assessing settleability and uniformity of the lithium ion battery anode slurry according to relative standard deviation of the solid contents. The method has the advantages of simple processes, convenient operation, good reappearance, accurate data and high analysis efficiency and can be widely used in industries.

Description

technical field [0001] The invention relates to the field of lithium-ion battery manufacturing, in particular to a method for evaluating the sedimentation and uniformity of the positive electrode material slurry of the lithium-ion battery. Background technique [0002] Especially in today's period when new energy vehicles are attracting much attention, lithium-ion batteries are more and more widely used; the preparation method of lithium-ion battery cathode material slurry is to mix the main components, such as lithium iron phosphate, conductive agent, binder Add solvents, solvents, etc. to the mixer in turn. Due to the large differences in physical properties such as specific gravity and specific surface among various materials, even if pre-mixed with a mixer in advance, it is difficult to prepare the lithium-ion battery cathode material slurry evenly, and it is prone to sedimentation and unevenness. Uniformity, resulting in poor consistency of the coated pole piece, result...

Claims

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Application Information

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Patent Type & AuthorityPatents(China)
IPC IPC(8): G01N5/04G01N15/04
Inventor尚伟丽孔令涌黄永侃
OwnerSHENZHEN DYNANONIC