Method of detecting residual quantity of hexaconazole in rice
A technology of hexaconazole and a detection method, which is applied in the field of detecting hexaconazole residues in rice, can solve the problems such as no method for detecting hexaconazole residues, and achieves the effects of good accuracy and precision and simple operation.
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[0013] The preferred embodiments of the present invention are described in detail below, so that the advantages and features of the present invention can be more easily understood by those skilled in the art, so as to define the protection scope of the present invention more clearly.
[0014] Embodiments of the invention include:
[0015] A method for detecting hexaconazole residues in rice, the detection method comprising the steps of:
[0016] b. Purification: Accurately absorb 10mL of the upper liquid phase after standing and stratifying, then dissolve the residue with 2mL n-hexane, pour n-hexanol and the dissolved residue into the pretreated silica solid-phase extraction column, and finally 15mL eluent For rinsing, use nitrogen gas to blow the n-hexane solution with residue and eluent to 3mL;
[0017] c. Detection: a. Sample extraction: Weigh 5g of prepared rice and place it in a conical flask, add 20mL of distilled water and 30mL of acetonitrile mixed extract, cover with...
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