Paint composition and multi-layer coating forming method
A multi-layer coating film and composition technology, which is applied in chemical instruments and methods, coatings, layered products, etc., can solve the problems of insufficient appearance of multi-layer coating films, and achieve excellent concealment, smoothness and vivid image Excellent performance and excellent weather resistance
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[0201] Example
[0202] Examples and comparative examples are listed below to further specifically describe the present invention. However, the present invention is not limited only to these examples. It should be noted that "parts" and "%" are obtained on the basis of quality.
[0203] Production of hydroxyl-containing acrylic resin (I-1)
Example Embodiment
[0204] Manufacturing example 1
[0205] In a reaction vessel equipped with a thermometer, a thermostat, a stirring device, a reflux condenser and a dripping device, 70.7 parts of deionized water and "Aクアロソ KH-10" (trade name, manufactured by Daiichi Kogyo Pharmaceutical Co., Ltd., emulsifier, effective Composition 97%) 0.52 parts, stirred and mixed in a nitrogen stream, and heated to 80°C. Next, 1% of the total amount in the following monomer emulsion and 5 parts of 6% ammonium persulfate aqueous solution were introduced into the reaction vessel and kept at 80°C for 15 minutes. Then, the remaining monomer emulsion was added dropwise to the reaction vessel kept at the same temperature over 3 hours. After the dropwise addition was completed, it was matured for 1 hour, and then 40 parts of 5% 2-(dimethylamino)ethanol aqueous solution was slowly added. It was added to the reaction vessel while cooling to 30°C, filtered with 100 mesh nylon cloth, and discharged at the same time to ob...
Example Embodiment
[0207] Manufacturing example 2
[0208] In a reaction vessel equipped with a thermometer, a thermostat, a stirring device, a reflux condenser and a dripping device, add 130 parts of deionized water and 0.52 parts of "Aクアロソ KH-10", stir and mix in a nitrogen stream, and heat up to 80°C . Next, 1% of the total amount in the following monomer emulsion (1) and 5.3 parts of 6% ammonium persulfate aqueous solution were introduced into the reaction vessel and kept at 80°C for 15 minutes. Then, the remaining monomer emulsion (1) was added dropwise to the reaction vessel kept at the same temperature over 3 hours, and aged for 1 hour after the dropwise addition was completed. Then the following monomer emulsion (2) was added dropwise over 1 hour, and after aging for 1 hour, 40 parts of 5% dimethylethanolamine aqueous solution was slowly added to the reaction vessel while cooling to 30°C, and filtered with 100 mesh nylon cloth , And discharged at the same time to obtain an average particl...
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