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45 results about "Dimethylethanolamine" patented technology

Dimethylethanolamine (DMAE or DMEA) is an organic compound with the formula (CH₃)₂NCH₂CH₂OH. It is bifunctional, containing both a tertiary amine and primary alcohol functional groups. It is a colorless viscous liquid. It is used in skin care products. It is prepared by the ethoxylation of dimethylamine.

Antistatic polyester fiber and preparation method thereof

The invention discloses an antistatic polyester fiber and a preparation method thereof, and relates to the field of fibers. When the antistatic polyester fiber is prepared, N, N-dimethylethanolamine reacts with allyl chloride, and then dichloro phthalocyanine silicon is grafted to obtain modified silicon phthalocyanine; polymerizing terephthalic acid, itaconic acid and ethylene glycol, and reacting with fluorescein isothiocyanate and modified silicon phthalocyanine in sequence to obtain modified polyester chips; the preparation method comprises the following steps: reacting phosphonitrilic chloride trimer with 3-hydroxy-5-nitropyridazine, and reducing to obtain a flame retardant; and carrying out melt spinning on the modified polyester chips and a flame retardant, and reacting to obtain the antistatic polyester fiber. The antistatic polyester fiber prepared by the invention has excellent antistatic property, antibacterial property, flame retardance and mechanical property.
Owner:SICHUAN BANGWEI HI-TECH SPECIAL TEXTILE CO LTD

High-performance thin film for automobile touch screen and preparation method of high-performance thin film

The invention discloses a high-performance film for an automobile touch screen and a preparation method of the high-performance film, and relates to the technical field of touch screen films. According to the preparation method, 3-chloropropyltriethoxysilane reacts with N, N-dimethylethanolamine, quaternary ammonium salt groups are introduced to nano silicon dioxide particles, the nano silicon dioxide particles are endowed with antistatic and antibacterial activity, then through polycondensation and hydrolysis reaction of vinyltriethoxysilane, the dispersity and compatibility of the nano silicon dioxide particles in a polymer are improved, the mechanical strength of a coating is enhanced, agglomeration is avoided, and the anti-static and antibacterial properties of the coating are improved. Meanwhile, constructing a photo-crosslinking network by using polyethylene glycol diacrylate; the copolymer contains fluorine, hindered amine and other groups, and forms another network through the cross-linking agent to provide an anchoring frame for functional groups, so that the coating realizes long-acting synergy of antistatic, anti-ultraviolet, anti-fingerprint and other functions in an automobile environment.
Owner:HUNAN XINGYUE TECH CO LTD

A waterborne polyurethane and its neutralization preparation method and application

This invention relates to the field of polymer materials, and specifically discloses a waterborne polyurethane, its neutralization preparation method, and its applications. This waterborne polyurethane is prepared by mixing the following raw materials in parts by weight: 10-30 parts by weight of a polyurethane prepolymer containing carboxyl functional groups, 5-25 parts by weight of a polyurethane prepolymer containing amino functional groups, 0.6-2.0 parts by weight of an organic amine chain extender, and 50-80 parts by weight of deionized water; wherein the polyurethane solid content accounts for 20-50% of the total weight of the raw materials. The preparation process of this invention is simple, the product is stable during storage, and it does not contain volatile or migrating amine neutralizing agents such as triethylamine or dimethylethanolamine, thus meeting the stringent regulatory requirements for applications such as food contact materials.
Owner:LELING SISHENG POLYMER MATERIALS CO LTD

Preparation method and application of a solid supported deep eutectic solvent material

This invention discloses a method for preparing and applying a solid-supported eutectic solvent material. The specific preparation process involves: firstly, chemically bonding a hydrogen bond acceptor derivative, N,N-dimethylethanolamine, onto the surface of a chloromethyl polystyrene resin support to generate a hydrogen bond acceptor structure in situ; then, thoroughly mixing this structure with a corresponding hydrogen bond donor, urea, to finally obtain the chloromethyl polystyrene resin-supported eutectic solvent material. The solid-supported eutectic solvent material provided by this invention combines the advantages of eutectic solvents and solid supports, overcoming the drawbacks of eutectic solvents such as easy loss during use, large dosage, and poor physical stability. It features a simple synthesis method, fast adsorption rate, and large adsorption capacity, and can be used for the efficient adsorption and removal of indomethacin sodium from water.
Owner:NORTH CHINA UNIV OF WATER RESOURCES & ELECTRIC POWER

Acrylic acid-organosilicone dual-modified polyester aqueous dispersion and preparation method thereof

The invention relates to an acrylic acid-organic silicon dual-modified polyester aqueous dispersion, which is prepared from the following components in percentage by weight: 1 to 5 parts of hexahydrophthalic anhydride, 10 to 15 parts of isophthalic acid, 1 to 5 parts of adipic acid, 15 to 20 parts of neopentyl glycol, 0.5 to 1 part of unsaturated binary acid, 1 to 2 parts of reflux solvent, 5 to 10 parts of acrylate mixed monomer, 0.5 to 1 part of acrylic acid, 5 to 10 parts of cosolvent, 1 to 5 parts of organic silicon modifier, 0.5 to 5 parts of dimethylethanolamine neutralizer and 40 to 45 parts of deionized water. The acrylic acid and the organic silicon are used for modifying the polyester at the same time, the weather resistance, the hydrolysis resistance and the adhesive force are remarkably improved while the high flexibility of the water-based polyester is kept, the synthesized water-based polyester dispersion can be used for preparing high-performance water-based coil steel coating or coil aluminum coating or other water-based amino coating with VOC smaller than or equal to 100 g / L, and good comprehensive performance is achieved.
Owner:深圳市深赛尔股份有限公司

Modified polyurethane water-based functional coating and preparation process thereof

The application discloses a modified polyurethane water-based functional coating and a preparation process thereof, and belongs to the technical field of water-based functional coatings. In the application, N,N-dimethylethanolamine is used as a blocking agent to block the isocyanate prepolymer, so that a latent type blocked isocyanate water-based polyurethane emulsion is prepared; lactide monomers, epoxy group grafted modified nano silicon dioxide and amino functionalized light stabilizer microcapsules are added into the emulsion; curing is carried out by using a two-stage process, that is, after preheating and water removal and film formation, 130-150 DEG C baking is carried out to trigger the deblocking of the DMEA blocked isocyanate, and the tertiary amine groups in the deblocked DMEA molecules immediately initiate the ring-opening polymerization of the premixed lactide monomers in the system in situ to generate polylactic acid segments which are chemically grafted to the crosslinked network. The application realizes the synchronous linkage of crosslinking and curing and polymer toughening, and the obtained coating has the characteristics of high crosslinking density, excellent flexibility and low internal stress.
Owner:ZHENJIANG YONGYI NEW MATERIAL TECH CO LTD

An electronic potting compound for packaging new energy power systems and its preparation method

This invention discloses an electronic potting compound for encapsulating new energy power systems and its preparation method, belonging to the field of adhesive preparation technology. The electronic potting compound for encapsulating new energy power systems consists of component A and component B. Component A includes polypropylene glycol, dicyclohexylmethane diisocyanate, hydroxyl-terminated polydimethylsiloxane, bismuth-zinc composite catalyst, N,N-dimethylethanolamine, porous alumina supported filler, composite halogen-free flame retardant, thixotropic agent, defoamer, and surface-modified calcium sulfate whisker fibers. Component B includes polypropylene glycol and dicyclohexylmethane diisocyanate. The electronic potting compound prepared by this invention exhibits good thermal conductivity and electromagnetic shielding capabilities after curing, while also possessing high mechanical strength.
Owner:SHANDONG WOSAI NEW MATERIALS TECHNOLOGY CO LTD

Amine solvent-based carbon capture compositions

A composition for carbon dioxide (CO2) capture includes 2-aminocyclohexanol, cis-1,2-diaminocyclohexane, meglumine, or combinations thereof. A process of CO2 capture includes mixing a CO2-containing gas with the composition. A system includes a component for receiving a gas and the composition, which absorbs CO2 from the gas. A further composition includes a first amine solvent selected from 2-aminocyclohexanol, cis-1,2-diaminocyclohexane, and meglumine and a second amine solvent independently selected from 2-aminocyclohexanol, cis-1,2-diaminocyclohexane, meglumine, ethyl diethanolamine, dimethylethanolamine, piperidine, 2-amino-2-methyl-1-propanol, and monoethanolamine. A further process includes reacting CO2 with an amine selected from 2-aminocyclohexanol, cis-1,2-diaminocyclohexane, and meglumine.
Owner:INTERNATIONAL BUSINESS MACHINE CORPORATION

Alkaline composition, its use and a process for cleaning substrates comprising cobalt and copper

The presently claimed invention relates to an alkaline composition for cleaning a substrate comprising i) copper or copper alloy and ii) cobalt or cobalt alloy, the composition comprising: a) at least one pH adjustor selected from diglycolamine, 4,4-diethoxy-N,N-dimethyl-1-butanamine, 3-dimethylaminopropan-1-ol, dimethylaminoethoxyethanol, N,N-dimethylisopropanolamine, ethylethanolamine, N-methyldiethanolamine, 2-(2-(methylamino)ethoxy)ethanol, 3-(methylamino)propane-1,2-diol, 2-[2-[2-(2-methoxy- ethoxy)ethoxy]ethoxy]ethylamine, 2-[2-(2-aminoethoxy)-ethoxy]-ethanol, N-butyldiethanolamine, diisopropanolamine, N-methyldiisopropanolamine, monoethanolamine, 3-dimethylamino-1,2-propandiol, 2- amino-1-butanol, 2-(2-(2-(2-aminoethoxy)ethoxy)ethoxy)ethanol, prolinol, 1-methyl-2-pyrrolidinemethanol, 1-methyl-2-pyrrolidinemethanol, 1-methyl-3-pyrrolidinol, 2-amino-2-methyl-1-propanol, N,N-dimethylethanolamine, butylethanolamine, diethylethanolamine, 3-methoxypropylamine, 4-(2-hydroxyethyl)morpholine, 4-(dimethylamino)cyclohexanol, 2-amino-2-methyl-1, 3-propanediol, or diisopropylamine; b) at least one complexing agent selected from C2 to C12 hydrocarbon having at least two sulfonic acid or carboxylic acid groups; c) at least one polymeric dispersing agent having a weight average molecular weight ≥ 1000 g / mol; and d) a solvent comprising water.
Owner:BASF SE

Cross-linking agent and preparation method of high-durability antistatic spandex fabric

The invention discloses a cross-linking agent and a preparation method of a high-durability antistatic spandex fabric, and the cross-linking agent is prepared by fully dissolving 20-30 parts of 4, 4 '-diphenylmethane diisocyanate in 200 parts of an organic solvent, adding 1-2 parts of dimethylethanolamine, and uniformly mixing. According to the high-durability antistatic spandex fabric, the spandex fabric passes through a padding machine containing a compression roller groove containing the cross-linking agent at the speed of 20-40 m / min, and the roller pressure is adjusted so that the liquid carrying rate of the spandex fabric can be 60%-80%; the spandex fabric subjected to padding treatment is fed into a continuous drying machine for partitioned drying, the linear speed of the spandex fabric in the continuous drying machine is controlled to range from 30 m / min to 50 m / min, and the standing time ranges from 2 min to 3 min; sequentially carrying out water washing and alcohol washing on the dried spandex fabric, carrying out low-temperature drying under the condition of 50-80 DEG C, and carrying out sizing and rolling to obtain the spandex fabric. According to the scheme, the problems of discontinuous antistatic property and poor antistatic durability of the spandex fabric in a stretching state can be solved.
Owner:NINGXIA NINGDONG TAIHE NEW MATERIAL CO LTD

Medical self-shedding water-based photocuring pressure-sensitive adhesive and preparation method thereof

The invention relates to a medical self-shedding water-based light-cured pressure-sensitive adhesive. The pressure-sensitive adhesive is prepared from the following raw material components: water-based light-cured polyurethane, a photoinitiator, a neutralizer, a reactive diluent and water, the neutralizing agent is one or more of dimethylethanolamine, triethylamine, triethanolamine and ammonia water; the active diluent is one or more of acryloyl morpholine, hydroxyethyl acrylate, hydroxyethyl methylacrylate, hydroxypropyl acrylate, hydroxybutyl acrylate, polyethylene glycol 400 dimethacrylate and polyethylene glycol 600 dimethacrylate; the initiator is a mixture of an initiator and a solvent; the water-based light-cured polyurethane is prepared from the following raw material components: diisocyanate, self-made polyol, a catalyst 1, a polymerization inhibitor and an end-capping reagent. According to the medical self-shedding water-based photocuring pressure-sensitive adhesive and the preparation method thereof, the pressure-sensitive adhesive has good initial viscosity, and after the pressure-sensitive adhesive is pasted on an affected part for a period of time, the initial viscosity and the holding power can be weakened until basically disappear, and the pressure-sensitive adhesive is easy to shed from skin without damaging the skin.
Owner:ZHEJIANG FENGLING NEW MATERIAL TECH CO LTD

Rubber modified emulsified asphalt as well as preparation method and application thereof

The invention discloses rubber modified emulsified asphalt as well as a preparation method and application thereof. The rubber modified emulsified asphalt comprises latex, petroleum asphalt, an ammonium salt emulsifier and a nonionic emulsifier, wherein the ammonium salt emulsifier is obtained by reacting vegetable oleic acid with N, N-dimethylethanolamine. The rubber modified emulsified asphalt disclosed by the invention can be used as a main raw material of a waterproof coating for buildings and roads and bridges, can improve the tensile strength, elongation at break, low-temperature flexibility, bonding strength, tear strength and other properties of the waterproof coating, can reduce the comprehensive cost, and can also be directly used as the waterproof coating for buildings and roads and bridges.
Owner:CHEMCHINA ZHUZHOU RUBBER RES & DESIGN INST

Efficient preparation method of tetracaine

The invention discloses an efficient preparation method of tetracaine, which comprises the following steps: 1, reacting para aminobenzoic acid, 1-bromobutane and triethylamine, concentrating under reduced pressure, adding an organic solvent and water, performing hot extraction and liquid separation, cooling an organic phase to separate out a solid, adding an acidic aqueous solution, cooling to crystallize, filtering and drying to obtain 4-butyl aminobenzoic acid butyl ester; 2, 4-butylaminobenzoic acid butyl ester, water, alcohol and sodium hydroxide are subjected to a reaction; decompressing and concentrating to remove the solvent, adding water for dissolving, acidifying with hydrochloric acid to separate out a solid, filtering and drying to obtain 4-butylaminobenzoic acid; 3, 4-butylaminobenzoic acid, N, N-dimethylethanolamine, a condensing agent or a hydroxyl activating agent and a reaction organic solvent react; adding an alkaline aqueous solution for washing and liquid separation, carrying out vacuum concentration on an organic phase, adding a refining solvent into a concentrate, heating, adsorbing with activated carbon, cooling for crystallization, filtering and drying to obtain a tetracaine finished product; the reaction temperature can be reduced, and the energy consumption is low; and the obtained product has high purity and high yield.
Owner:JIANGSU YINGKE BIOPHARMACEUTICAL CO LTD

Water-based acrylic resin-based rotor antirust agent and processing method thereof

The invention relates to the technical field of antirust agents, in particular to a water-based acrylic resin-based rotor antirust agent and a processing method thereof. The water-based acrylic resin-based rotor antirust agent is prepared from the following raw materials in parts by weight: 50 to 60 parts of modified acrylic resin, 10 to 20 parts of deionized water, 0.1 to 0.2 part of dimethylethanolamine, 4 to 6 parts of barium sulfate, 10 to 15 parts of mica iron oxide, 0.1 to 0.3 part of dispersing agent, 0.1 to 0.2 part of defoaming agent, 0.1 to 0.3 part of flatting agent and 1 to 3 parts of coalescing agent. The antirust agent A and the antirust agent B are combined in the water-based acrylic resin to play a synergistic role, so that the water-based acrylic resin-based rotor antirust agent with excellent antirust property and adhesive force is prepared, and meanwhile, the water-based acrylic resin-based rotor antirust agent has excellent corrosion resistance and hydrophobicity.
Owner:DONGGUAN YINGFEITE LUBRICATION TECH CO LTD

Electronic pouring sealant for packaging new energy power system and preparation method of electronic pouring sealant

The invention discloses an electronic pouring sealant for packaging a new energy power system and a preparation method of the electronic pouring sealant, and belongs to the technical field of adhesive preparation. The invention relates to an electronic pouring sealant for packaging a new energy power system, which is composed of a component A and a component B. The component A comprises the following raw materials: polypropylene glycol, dicyclohexylmethane diisocyanate, hydroxyl-terminated polydimethylsiloxane, a bismuth-zinc composite catalyst and N, N-dimethylformamide. The flame retardant is prepared from N, N-dimethylethanolamine, porous aluminum oxide loaded filler, a composite halogen-free flame retardant, a thixotropic agent, a defoaming agent and surface-modified calcium sulfate whisker fibers. The component B is prepared from the following raw materials: polypropylene glycol and dicyclohexylmethane diisocyanate. The prepared electronic pouring sealant has good heat conduction capability and electromagnetic shielding capability after being cured, and also has relatively high mechanical strength.
Owner:SHANDONG WOSAI NEW MATERIALS TECHNOLOGY CO LTD

Epoxy modified polyurethane coating and preparation method thereof

The invention discloses an epoxy modified polyurethane coating and a preparation method thereof, and belongs to the technical field of coatings. The preparation method of the epoxy modified polyurethane coating comprises the following steps: mixing epoxidized oil, deionized water and 2-methyl-2-propanol, heating and refluxing at 50-70 DEG C for 20-40 minutes, then adding phosphoric acid, reacting at 80-100 DEG C for 5-7 hours, dissolving the product in ethyl acetate, separating out an organic layer, washing and drying to obtain phosphorus-containing polyol; the preparation method comprises the following steps: mixing phosphorus-containing polyol, isocyanate and 1, 6-hexanediol, introducing inert gas, stirring at 60-80 DEG C for 3-4 hours, adding a diluent, and cooling to room temperature to obtain a prepolymer; and adding N, N-dimethylethanolamine into the prepolymer, stirring for 20-40 minutes, then adding epoxy silane modified cellulose nanocrystals, then adding deionized water, stirring, and removing the diluent in vacuum to obtain the epoxy modified polyurethane coating with the solid content of 20-40 wt%. And the coating has good water resistance, corrosion resistance and mechanical properties, so that the barrier property of the coating is improved, and the corrosion resistance is greatly improved.
Owner:WEIFANG HONGYUAN WATERPROOF MATERIAL

Production method of N, N-dimethylethanolamine

The invention relates to a production method of N, N-dimethylethanolamine, and belongs to the technical field of organic compound preparation. The problems of high energy consumption, low product yield, more impurities and the like of the preparation method of N, N-dimethylethanolamine in the prior art are solved. According to the production method disclosed by the invention, the compound ionic liquid is used as a catalyst to catalyze the reaction of ethylene oxide and dimethylamine to obtain N, N-dimethylethanolamine. According to the production method, the composite ionic liquid is adopted as the catalyst, so that the production energy consumption is reduced, the EO conversion rate and the DMEA selectivity are obviously improved, the product has few impurities and high purity which is not less than 99.98%, the problems that the catalyst is not easy to recycle and separate and the like are solved, and a good effect is achieved.
Owner:HEBEI UNIV OF TECH

Ultraviolet curing asphalt pavement cold patch material

The invention relates to the technical field of pavement materials, in particular to an ultraviolet light curing asphalt pavement cold patch material which is composed of cold patch liquid and aggregate, the mass ratio of the cold patch liquid to the aggregate is (4-6): 100, the cold patch liquid comprises decolorized asphalt and an ultraviolet light curing resin system, and the ultraviolet light curing resin system comprises a curing agent and a curing agent. The mass ratio of the decolorized asphalt to the ultraviolet curing resin system is 100: (10-30), and the ultraviolet curing resin system is prepared from the following components in parts by mass: 50 to 70 parts of epoxy acrylate resin, 20 to 40 parts of tripropylene glycol diacrylate, 2 to 5 parts of 2, 4, 6-trimethylbenzoyl-diphenyl phosphine oxide and 0.5 to 1 part of dimethylethanolamine. The problems that a traditional cold patch material is long in curing time and slow in strength forming are solved, a specific ultraviolet curing resin system and decolorized asphalt are adopted, rapid curing is conducted under the illumination condition, high strength is provided for pavement pit slot repairing, vehicle loads can be effectively borne, the durability of a repaired pavement is enhanced, and the requirement for rapid traffic opening is met.
Owner:TIANJIN CHENGJIAN UNIV

Two-component self-emulsifying polyester acrylic acid dispersion and preparation method thereof

PendingCN121378600APolyesterHydrophilic monomer
The invention discloses a two-component self-emulsifying polyester acrylic dispersion and a preparation method thereof, and relates to the field of waterborne polyurethane paints.The preparation method comprises the following steps that a half ester intermediate is prepared and reacts with ethylene carbonate, and a hydrophilic monomer with cyclic carbonate groups is obtained; dibasic acid and dihydric alcohol are subjected to polycondensation to obtain initial resin, propylene glycol monomethyl ether, a mixed solution a containing hydrophilic monomers and a mixed solution b are added into the initial resin at intervals, mixing is conducted, and functional resin is obtained; the functional resin and dimethylethanolamine are subjected to a stirring reaction, then deionized water is added, mixing is conducted, and a product with the D50 being 50-150 nm and the PDIlt is obtained; and 0.2 of a two-component self-emulsifying polyester acrylic acid dispersion. According to the preparation method disclosed by the invention, the hydrophilic monomer with a cyclic carbonate group is introduced during preparation, and a step-by-step controlled polycondensation and graft polymerization process is adopted, so that the hydrophilic monomer is directionally and uniformly anchored on a polyester main chain, and the problem of non-uniform molecular structure caused by random copolymerization of the hydrophilic monomer in a traditional method is avoided.
Owner:HUIZHOU SHEN SAIER CHEM CO LTD

Water-based Teflon non-stick coating and preparation method thereof

The invention discloses a water-based Teflon non-stick coating and a preparation method thereof, and belongs to the technical field of coatings, the water-based Teflon non-stick coating comprises the following raw materials by weight: 1.5-2% of a thickener, 0.8-1.3% of dimethylethanolamine, 2.5-4.2% of pearl powder, 3-5% of an adhesion promoter, 25.3-31.3% of deionized water, 1-2% of carbon black, 0.4-1.2% of a wetting agent, 0.5-1% of a leveling agent, 1.8-2.3% of wear-resistant powder, and 1-5% of a hardening agent. The balance is polytetrafluoroethylene emulsion. Through the mode, the prepared water-based Teflon single-layer non-stick coating does not need to be sprayed for the second time, the coating has high abrasion resistance, meanwhile, the surface of the coating is good in anti-adhesion performance, and the adhesive force between the coating and the surface of a base body is high.
Owner:CHANGZHOU TENGCHEN CHEMICAL CO LTD

Method for preparing high-weather-resistance solvent-free polyurethane from polycarbonate diol

The invention relates to the technical field of water-based paint preparation, and discloses a method for preparing high-weather-resistance solvent-free polyurethane from polycarbonate diol. The water-based paint is prepared from BF-8021 water-based ultrafast-drying anticorrosive resin, BF-9011 acrylic dispersion, a dispersing agent special for carbon black, carbon black, light calcium carbonate, barium sulfate, dimethylethanolamine, propylene glycol monomethyl ether, a defoaming agent, an anti-settling agent special for water-based paint, a drier special for water-based paint, texanol and water. The coating prepared by the invention has ultrafast drying speed, the drying speed of paint film surface drying is 10 minutes, and the hard drying time is 40 minutes; the paint film does not rust or fall off after the neutral salt spray test is carried out for 200h; after the paint is artificially aged for 200 hours, the paint film does not have the phenomena of cracking, powdering, bubbling, falling and rusting, the color difference E is 2.9, the gloss loss rate after water washing is 28%, the gloss loss rate after polishing is 8%, and the requirements that the cast pipe paint does not rust, does not lose gloss, does not fall off and the like after being stored outdoors for 2 years are met.
Owner:XINJIANG QIANGRUN PAINT CO LTD

Water boiling heating plate coating

The invention discloses a water boiling heating plate coating which comprises a primer layer and a finish paint layer, the finish paint layer is located above the primer layer, and pores are formed in the finish paint layer. The primer layer comprises the following components in parts by weight: 15-20 parts of adhesive resin, 1-3 parts of amorphous silicon dioxide, 2-5 parts of silicon carbide, 0.5-1 part of dimethylethanolamine, 5-8 parts of polytetrafluoroethylene, 10-15 parts of a high-temperature solvent, 0.2-0.5 part of a water-based additive and 55-65 parts of deionized water. The finish paint layer comprises the following components in parts by weight: 8-10 parts of polyether sulfone, 10-15 parts of mica, 2-5 parts of a water-based additive and 70-90 parts of deionized water. When the coating is in contact with water, a small amount of bubbles can be remained on the surface of the primer layer at the joint of the primer layer and the finishing coat layer; in the heating process, bubbles on the surface of the primer layer expand, are extruded by capillary holes and are separated from the coating to form a large number of tiny bubbles, the small bubbles release heat in the floating process in water, the heat conduction efficiency is improved, the heating efficiency of the water boiler is improved, and noise is reduced.
Owner:ANMUSEN NEW MATERIAL CO LTD SHUNDE DISTRICT FOSHAN CITY

A kind of synthetic method of tetracaine

The present invention relates to a method for synthesizing tetracaine, comprising the steps of: using N-Boc-4-aminobenzoic acid (A) as a raw material, and reacting with n-butyl bromide to obtain N-Boc-N-butyl-4-aminobenzoic acid butyl ester (B); removing Boc from N-Boc-N-butyl-4-aminobenzoic acid butyl ester (B) under weak acid to obtain N-butyl-4-aminobenzoic acid butyl ester (C); and reacting N-butyl-4-aminobenzoic acid butyl ester (C) with N,N-dimethylethanolamine to obtain tetracaine (I). This method effectively reduces the risk of generating N-disubstituted butyl impurities, does not require palladium-carbon hydrogenation, and the purity and yield of the prepared tetracaine are both high, the product purity is greater than 99.8%, and the single impurity is less than 0.05%, which meets the requirements of medicinal raw materials.
Owner:SHANDONG CHUANGXIN PHARMA RES & DEV

A rare earth-selenium tungsten oxide nanocluster material functionalized with hybrid organic ligands, its preparation method and application

This invention relates to a rare-earth-selenium tungsten oxide nanocluster material functionalized with mixed organic ligands, the chemical formula of which is [HDMEA]. 9 Na 12 H3[Ce6(DMEA)3(H2O)9W9(HTA)6O 18 (SeW9O 33 [6]ˑ81H2O, where DMEA = N,N-dimethylethanolamine and H3TA = hydroxymalonic acid. This material is prepared by a one-step self-assembly reaction of sodium tungstate dihydrate, N,N-dimethylethanolamine, sodium selenite, hydroxymalonic acid, and cerium nitrate hexahydrate in aqueous solution. The experimental operation is simple and the cost is low. This material can be used as a polyanionic polymer to form a thin film material by layer-by-layer assembly with positively charged chitosan. This multilayer film can be used as a sensitizing material to combine with polypyrrole containing template molecules (2,4-dichlorophenol) to form a molecularly imprinted polymer. This polymer can be used to construct an electrochemical sensor for detecting 2,4-dichlorophenol. Experimental results show that this electrochemical sensor has high sensitivity, strong stability, a wide detection range (1 μM–1 mM), and a low detection limit (0.125 μM).
Owner:HENAN UNIVERSITY

Grinding aid for efficiently preparing limestone powder and preparation method of grinding aid

The invention discloses a grinding aid for efficiently preparing limestone powder and a preparation method of the grinding aid, and belongs to the technical field of limestone powder preparation. The grinding aid is prepared from the following raw materials: 10-30 parts of phosphate amine salt, 1-5 parts of sodium n-alkyl benzene sulfonate, 1-3 parts of ionic liquid, 1-5 parts of La < 3 + > doped CeO2 nanoparticles, 1-3 parts of a permeation component, 5-15 parts of a dispersion component and 40-80 parts of water. Wherein the phosphate amine salt is dodecyl phosphate diethanolamine salt, the linear alkyl sodium benzene sulfonate is sodium tetradecyl benzene sulfonate, the ionic liquid is 1-butyl-3-methylimidazole bis (trifluoromethanesulfonyl) imide salt, the permeation component is sec-octyl alcohol polyoxyethylene ether, and the dispersion component comprises dipropylene glycol and dimethylethanolamine. The invention relates to 2-amino-2-methyl-1-propanol and a preparation method thereof. According to the grinding aid disclosed by the invention, through the synergistic effect of various components, the grinding aid is fully mixed with limestone and permeates into surface gaps of the limestone, so that the surface tension is effectively reduced, the crack propagation is promoted, the limestone powder fineness is improved, the grinding efficiency is improved, and the grinding energy consumption is reduced.
Owner:SHANDONG HONGYI TECH +1

Baking type water-based single-component acrylic acid effect pigment coating and preparation method thereof

The invention relates to the field of water-based paint, and particularly discloses baking type water-based single-component acrylic acid effect pigment paint and a preparation method thereof. The baking type water-based single-component acrylic acid effect pigment coating is prepared from the following raw materials in percentage: 55 to 65 percent of acrylic acid core-shell emulsion, 1 to 2 percent of N, N-dimethylethanolamine, 1 to 5 percent of partially methylated amino resin, 1 to 5 percent of ethylene glycol butyl ether, 1 to 3 percent of dipropylene glycol butyl ether, 10 to 15 percent of absolute ethyl alcohol, 1 to 4 percent of auxiliaries, 6 to 10 percent of effect pigment and the balance of water. The acrylic core-shell emulsion and the amino resin are cross-linked to form a compact network structure, so that directional arrangement of the effect pigment is promoted, the phenomena of floating and spots of the pigment on the surface of a coating are reduced, and the directional effect of the effect pigment in the coating is improved.
Owner:CHANGZHOU HUALING NEW MATERIAL CO LTD

Environment-friendly ceramic cement paint and preparation method thereof

The invention discloses environment-friendly ceramic cement paint. Comprising the following components in parts by weight: 100-120 parts of a polyurethane solution, 50-60 parts of ordinary Portland cement, 30-40 parts of a chitosan modified solution, 30-40 parts of a styrene-acrylic polymer emulsion, 10-15 parts of potassium tripolyphosphate, 1-3 parts of a polycarboxylate superplasticizer, 1-5 parts of dimethylethanolamine, 5-8 parts of barium metaphosphate, 13-18 parts of potassium chloride and 5-10 parts of dibutyl phthalate. 1 to 3 parts of cellulose ether; and 2 to 4 parts of polydimethylsiloxane. According to the environment-friendly ceramic cement paint and the preparation method thereof, the environment-friendly ceramic cement paint has excellent mechanical strength and high wear resistance.
Owner:FUJIAN DEHUA WANDA CERAMICS CO LTD

A glass fiber reinforced polyurethane composite door and window profile formed by injection impregnation pultrusion process and its processing technology and application

This application relates to a glass fiber reinforced polyurethane composite door and window profile formed using an injection-impregnation pultrusion process, as well as its processing technology and application. This application relates to the field of composite materials technology and can be used in the construction field, such as the preparation of doors and windows. The polyurethane material in this application comprises components A and B, with the injection mass ratio of components A and B being 100:(60-100). Component A comprises liquefied MDI, and component B comprises: 100 parts flame-retardant polyether polyol, 2-10 parts 1,4-butanediol, 2-10 parts calcium oxide, 0.3-0.5 parts dimethylethanolamine, 0.5-0.8 parts azobisisobutyronitrile, 0.5-1.5 parts trimethylsiloxysilicate, and 0.1-0.5 parts silicone defoamer. The water content of component B is controlled to be no more than 0.05wt%. This processing method can increase the glass fiber pulling speed while reducing the impact of bubbles, improve the thermal stress concentration problem of the profile product, and further enhance the vertical shear strength of the profile.
Owner:SHANDONG CHINA CONSTRUCTION EIGHTH BUREAU CARBON FIBER COMPOSITE MATERIALS CO LTD

Coating composition for metal packages for food, preparation method therefor, and metal packaging can

PCT designated stageWO2026086019A1Anti-corrosive paintsFood safetyCross linker
Provided in the present invention are a coating composition for metal packages for food, a preparation method therefor and a metal packaging can. Using 100 parts by weight of epoxy acrylate resin as reference, the composition of the present invention comprises: 10-25 parts by weight of dimethylethanolamine, 0.5-3 parts by weight of wax slurry, 5-10 parts by weight of a crosslinking agent, 0.1-1.1 parts by weight of a defoamer and 200-350 parts by weight of deionized water. The composition of the present invention enables a small coating amount, convenient use and high bubble storage capacity, and has environmental friendliness and food safety.
Owner:SHANGHAI BAOYIN METAL DECORATION

A water-based plastic baking paint with high aging resistance and preparation method thereof

The present invention discloses a water-based plastic baking varnish with high aging resistance and a preparation method thereof, relating to the technical field of water-based coatings. The present invention discloses a preparation method for a water-based plastic baking varnish, comprising the following steps: adding a water-based resin, N,N-dimethylethanolamine, and deionized water to a dispersion tank and uniformly dispersing the mixture; further adding isopropyl alcohol and a film-forming aid and uniformly dispersing the mixture; sequentially adding a wetting agent, a defoaming agent, and a thickener and uniformly dispersing the mixture; and filtering the mixture to obtain a water-based plastic baking varnish. The water-based resin prepared in the present application is obtained by copolymerizing a silica-modified epoxy resin with an acrylic resin. The water-based plastic baking varnish prepared in the present application has excellent aging resistance and good mechanical properties.
Owner:DONGGUAN RUIDA COATINGS CO LTD