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Linear type smoking machine collecting device with adsorption tube and analytical test method of collecting device

A technology of adsorption tube and smoking machine, which is applied in the direction of measuring devices, analysis materials, sampling devices, etc., can solve the problems of cumbersome operation, poor test result reproducibility, suction channel dead volume and large pressure drop, and achieve good adsorption Effect, prolonged residence time, effect of effective absorption

Active Publication Date: 2015-01-07
CHINA NAT TOBACCO QUALITY SUPERVISION & TEST CENT
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The cold solution absorption method uses two collection bottles in series with 15mL of cold methanol to collect, and the operation is cumbersome
Sorbent tube method, the "dead volume" and pressure drop of the suction channel of the smoking machine are large, and the reproducibility of the test results is poor

Method used

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  • Linear type smoking machine collecting device with adsorption tube and analytical test method of collecting device
  • Linear type smoking machine collecting device with adsorption tube and analytical test method of collecting device
  • Linear type smoking machine collecting device with adsorption tube and analytical test method of collecting device

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036]Select brand A cigarettes, perform sample balance according to the conditions specified in the GB / T 16447 standard, and select (average mass ± 0.02) g and (average draw resistance ± 50) Pa cigarettes for sample testing. Install the prepared trapping device on the smoking machine, and carry out suction under the conditions specified in the ISO standard, with a suction volume of 35.0 mL, a suction time of 2 s, and a suction frequency of 60 s. Aspirate 1 tube each time; remove the trapping device after suction and trapping, take out the adsorption tube, cut it open, and transfer it to the corresponding container for extraction treatment; make a blank sample in the same process, and compare the processing results of the blank sample with A Cigarette treatment results were compared.

[0037] Table 2A Determination results of volatile organic compounds in brand cigarettes-ISO

[0038]

Embodiment 2

[0040] Select brand B cigarettes, perform sample balance according to the conditions specified in the GB / T 16447 standard, and select (average mass ± 0.02) g and (average draw resistance ± 50) Pa cigarettes for sample testing. Install the prepared trapping device on the smoking machine, and smoke under the conditions specified in the Canadian Intensive Inhalation (HCI) standard, with a suction volume of 55.0 mL, a suction time of 2 s, and a suction frequency of 30 s. Aspirate 1 tube at a time; remove the trapping device after suction and trapping, take out the adsorption tube, cut it open, and transfer it to the corresponding container for extraction treatment; make a blank sample in the same process, and compare the processing results of the blank sample with the B Cigarette treatment results were compared.

[0041] Table 3 Determination results of volatile organic compounds in a certain brand of cigarettes-HCI

[0042]

[0043]

[0044] HCI: deep suction mode

[0045...

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Abstract

The invention provides a linear type smoking machine collecting device with an adsorption tube and an analytical test method of the collecting device. The linear type smoking machine collecting device with the adsorption tube comprises the adsorption tube (1), an artificial lip gripper (2), artificial lips (3), a collector front cover (5), a collector rear cover (7) and an adsorption tube holding member (8), wherein the artificial lips (3) are arranged inside the artificial lip gripper (2). According to the device, the operation is simple and convenient, the repeatability of assaying is good, the consumption of an organic solvent is low, the sample test result is free from significant difference from the sample test results of the standard methods, and the collection of volatile organic compounds can be realized at room temperature, so that the device is applicable to the analysis of large-batch samples.

Description

technical field [0001] The invention relates to the technical field of analysis and detection of cigarette smoke, in particular to a collection device of a linear smoking machine with an adsorption tube and a method for analyzing and testing cigarette smoke using the collection device. Background technique [0002] With the in-depth research on smoking and health, people are paying more and more attention to the harmful components in cigarette smoke. Cigarette mainstream smoke contains a large number of volatile organic compounds. Among the 44 harmful components listed on the Health Canada Concerned Detection List, there are 5 volatile organic compounds: 1,3-butadiene, isoprene, acrylonitrile, benzene and toluene. The carcinogenicity of 1,3-butadiene and isoprene is listed by IARC as a possible human carcinogen (2B); benzene is a human carcinogen, and its carcinogenicity is "sufficient data from animal experiments and human experiments" (Group1); IARC lists acrylonitrile a...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N1/24G01N33/00
Inventor 罗彦波李雪张洪非朱风鹏庞永强陈再根姜兴益侯宏卫胡清源黄卫东辛宝珺常诚曾波孟科
Owner CHINA NAT TOBACCO QUALITY SUPERVISION & TEST CENT
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