Method for determining content of methanol in air of work place
A workplace, methanol content technology, applied in measuring devices, instruments, scientific instruments, etc., can solve problems such as inability to automatically inject samples, water damage to chromatographic columns, etc., achieve long sample shelf life, high result stability, and reduce detection out-of-limit effect
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[0040] 1. Preparation of standard curve and others
[0041] (1), sampling
[0042] Use short-time sampling. At the sampling point, open both ends of the silica gel tube (GH-I solvent desorption type silica gel tube 6×12mm; 200mg / 100mg silica gel inside), and collect air samples for 15min at a flow rate of 100mL / min. The sampling volume is 1.5L. air sample. Immediately after sampling, seal both ends of the silicone tube with a plastic cap, put it in a clean container, store and transport at room temperature.
[0043] (2), instruments and reagents
[0044] Personal air sampler (Beijing Zhongxi Yuanda Technology Co., Ltd., model QR7-ZR3600);
[0045] Shimadzu GC-2010 gas chromatograph with hydrogen flame ionization detector (FID);
[0046] DANI 44 position automatic headspace sampler;
[0047] Methanol stock solution: add an appropriate amount of water to a 100ml volumetric flask, add a certain amount of methanol after accurate weighing, and then accurately weigh, make up to...
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