Method for preparing rosavin from rose rhodiola rosea
A technology of rose red and luoxiwei, which is applied to the preparation of sugar derivatives, chemical instruments and methods, sugar derivatives, etc., can solve the problems of unsatisfactory market demand, unstable health care function, and low purity of luoxiwei, and achieve Good impurity removal effect, simple steps and high yield
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[0027] (1) Weighing 200kg of dried Rhodiola rosea, the content of rosavirin and salidroside is 1.38%, and the content of salidroside is 0.92%, and it is crushed to 20 meshes; the mass ratio is 60% ethanol aqueous solution to extract and reflux three times, and the ratio of extraction solvent to material 8:1; 6:1; 4:1; the extraction time is 2 hours;
[0028] (3) Mix and concentrate the extracts, the vacuum degree is the vacuum concentration temperature is below 60°C, the vacuum degree is not less than 0.08pma, the concentration time is not more than 2 hours, and the concentration is concentrated to an alcohol-free state with a density of 1.05-1.10; (4 ) The concentrated solution is centrifuged with a filter cloth of 500 mesh;
[0029] (5) Pack the processed D101 macroporous resin into a 200L column. The centrifugate has an adsorption speed of 1.0-1.5bv / h and a water washing speed of 2-3 bv / h. Wash until the next column liquid is colorless and ethanol is eluted The concentra...
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