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Farmland irrigation water sampling method

A technology for farmland irrigation and farmland, applied in the field of heavy metal pollution monitoring in water, can solve problems such as inability to monitor, cannot be used on a large scale, and difficulty, and achieves the effects of simple sampling method, good sampling effect, and strong adsorption force.

Inactive Publication Date: 2015-10-14
农业部亚热带果品蔬菜质量监督检验测试中心
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Single sampling is the simplest, just use a container to directly take a certain amount of water for detection, but it has a major disadvantage: it can only reflect the situation at one point in time, it is almost ineffective for intermittent pollution, and it cannot be used for a period of time detected
The online collector works well, but its main disadvantage is that it is expensive and cannot be used on a large scale. It must also have fixed facilities, mains power supply and manual maintenance in order to run normally for a long time. It is suitable for monitoring pollution in industrial areas. For outdoor The applicability of the monitoring of vast farmland irrigation water is poor, and it is difficult to perform multi-point sampling and long-term sampling of farmland irrigation water
[0003] With the increasingly serious water pollution and the vigorous development of environmental monitoring and control of agricultural products, the existing monitoring and sampling work is difficult to meet the needs. It is very necessary to explore low-cost and long-term sampling methods for farmland irrigation water.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] A sampling method for farmland irrigation water, boiling 15 min with hydrochloric acid with a volume concentration of 10% and analytically pure activated carbon, purifying the activated carbon, filtering while hot, rinsing the activated carbon with pure water, drying the activated carbon, and setting aside. Weigh 10 g of purified activated carbon, put it into a small bag made of cloth material, which has micropores, and its pore size is smaller than the diameter of activated carbon particles, seal it, and press the bag to keep it flat to make an activated carbon absorption bag. The prepared activated carbon absorption pack was placed in a porous plastic bottle, and the plastic bottle was fixed on the sampling rod with nails to complete the installation of the sampler. Insert the sampling rod into the ditch of the irrigation water, adjust the height of the activated carbon absorption bag so that it is completely immersed in the water, do not let the soil cover the activat...

Embodiment 2

[0023] A sampling method for farmland irrigation water, boiling 10 min with sulfuric acid with a volume concentration of 20% and analytically pure activated carbon, purifying the activated carbon, filtering while hot, rinsing the activated carbon with pure water, drying the activated carbon, and setting aside. Weigh 10 g of purified activated carbon, put it into a small bag made of nylon mesh material, which has micropores, and its pore size is smaller than the diameter of activated carbon particles, seal it, and press the bag to keep it in a flat state to make activated carbon absorb Bag. The prepared activated carbon absorption pack was placed in a porous plastic bottle, and the plastic bottle was fixed on the sampling rod with nails to complete the installation of the sampler. Insert the sampling rod into the farmland ditch, adjust the height of the activated carbon absorption bag, make it completely immersed in the water, do not let the soil cover the activated carbon abso...

Embodiment 3

[0025] A sampling method for farmland irrigation water, boiling 15 min with nitric acid with a volume concentration of 15% and analytically pure activated carbon, purifying the activated carbon, filtering while hot, rinsing the activated carbon with deionized water, drying the activated carbon, and setting aside. Weigh 12 g of purified activated carbon, put it into a small bag made of cloth material, which has micropores, and its pore size is smaller than the diameter of activated carbon particles, seal it, and press the bag to keep it flat to make an activated carbon absorption bag. The prepared activated carbon absorption pack was placed in a porous plastic bottle, and the plastic bottle was fixed on the sampling rod through a rope to complete the installation of the sampler. Insert the sampling rod into the ditch of the irrigation water, adjust the height of the activated carbon absorption bag so that it is completely immersed in the water, do not let the soil cover the acti...

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PUM

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Abstract

The invention provides a farmland irrigation water sampling method including the procedures of activated carbon purification, activated carbon absorption bag preparation, sampler installation, sampling and target substance elution; activated carbon after purification is put into a small bag and sealed, an activated carbon absorption bag is prepared, the activated carbon absorption bag is mounted on a sampling rod to prepare a sampler, the sampler is placed in farmland or an irrigation water channel for sampling, a target substance in the activated carbon absorption bag taken from sampling is eluted, and a to-be-measured solution is obtained. The sampler produced with activated carbon as an adsorbent, has quite strong adsorption capacity on various heavy metals, has low cost, has the consistent adsorption capacity after being soaked in water for 30 days, and has the function of long-term accumulation adsorption acquisition of the target substance. The sampling method is simple and is convenient to operate, and provides a sampling method for the heavy metal total amount in water in a longer period for pollution monitoring and evaluation works of the farmland irrigation water.

Description

technical field [0001] The invention belongs to the field of heavy metal pollution monitoring in water, in particular to a sampling method for farmland irrigation water. Background technique [0002] In the monitoring of heavy metal pollution in environmental water, whether sample collection is effective is one of the key technical tasks of monitoring. At present, there are mainly two methods of single collection and online collection. Single sampling is the simplest, just use a container to directly take a certain amount of water for detection, but it has a major disadvantage: it can only reflect the situation at one point in time, it is almost ineffective for intermittent pollution, and it cannot be used for a period of time monitored. The online collector works well, but its main disadvantage is that it is expensive and cannot be used on a large scale. It must also have fixed facilities, mains power supply and manual maintenance in order to run normally for a long time....

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N1/10G01N1/28
Inventor 甘志勇彭靖茹农耀京李鸿蓝唯时鹏涛秦玉燕李乾坤王运儒
Owner 农业部亚热带果品蔬菜质量监督检验测试中心
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