Preparation method and application of water-soluble insect-resistant and mosquito-repellent plant oil
A vegetable oil and water-soluble technology, applied in the direction of botany equipment and methods, applications, pest repellents, etc., to achieve stable performance, avoid photolysis and oxidation, and improve environmental sanitation
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Embodiment 1
[0013] Preparation of citronella oil / hydroxypropyl-β-cyclodextrin inclusion compound: get 500 grams of hydroxypropyl-β-cyclodextrin, dissolve in 500ml95% ethanol, add 50ml citronella oil. Stir in a blender at 2000 rpm for 20 minutes. Ethanol was recovered by distillation at 60°C, and then vacuum-dried to obtain 534 g of dry powder of the clathrate. Take the clathrate and make a 10% aqueous solution to form a stable suspension. The formation of citronella oil / hydroxypropyl-β-cyclodextrin inclusion complex can be proved from the infrared spectrum 1.
Embodiment 2
[0015] The preparation of citronella oil / methylation-beta-cyclodextrin clathrate: get methylation-beta-cyclodextrin 500 grams, be dissolved in the ethanol of 500ml95%, and add 50ml citronella oil, in blender Stir and clathrate at 2000 rpm for 20 minutes. Ethanol was recovered by distillation at 60°C, and dried in vacuum to obtain 542 g of dry powder of the clathrate. Take clathrate and make 10% clear aqueous solution. The formation of citronella oil / methylated-β-cyclodextrin inclusion complex can be proved from the infrared spectrum 2.
Embodiment 3
[0017] Application of citronella oil / methylated-β-cyclodextrin inclusion complex:
[0018] Take citronella oil / methylated-β-cyclodextrin inclusion complex, mix it with 10% aqueous solution, pack it aseptically, and make it into a spray to repel mosquitoes and flies, which can be used indoors and on people's clothing or skin. Spray to repel mosquitoes. It is also possible to add peppermint oil or other essential oils to the water-soluble clathrate for flavoring, and it can be made into a spraying agent as above.
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