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Seven-into-one sulfanilamide detection method and kit

A detection method and kit technology, applied in the preparation of test samples, measuring devices, color/spectral characteristics measurement, etc., can solve the problems of high operational skill requirements, high cost, long detection time, etc., and achieve operational skills The effect of low requirements, low cost and short detection time

Inactive Publication Date: 2017-03-15
WUXI X RES PROD DESIGN & RES
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] Aiming at the deficiencies of the prior art, the present invention provides a seven-in-one sulfonamide detection method and a kit, which have common and cheap instruments in the seven-in-one sulfonamide detection, low operating skill requirements, relatively short detection time and low cost and other advantages, which solve the problems of expensive instruments, high requirements for operation skills, long detection time and high cost in the detection of sulfa seven-in-one

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] A seven-in-one detection method for sulfonamides, comprising the following steps:

[0025] S1. Synthesize the molecularly imprinted material of sulfonamide by bulk polymerization: 2 parts of sulfathiazole, 1 part of trimethoprim, 3 parts of sulfaquinoxaline, and 1 part of phthaloyl Sulfathiazole, 3 parts of sulfamethiadiazole, 4 parts of sulfamethazine, 12 parts of sulfamethoxazole, 7 parts of sulfamethazine, 3 parts of sulfamethoxine, 21 parts of sulfachloropyridazine carrier, 2 parts Mix one part of m-methoxine, 7 parts of sulfaquinoxaline, 9 parts of sulfadiazine, 1 part of sulfamethoxypyridazine and 2 parts of sulfamethoxine, and mix the mixed sulfathiazole, trimethoprim, and sulfamethoxine Quinoxaline, Phthalylsulfothiazole, Sulfamethiadiazole, Sulfamethazine, Sulfamethoxazole, Sulfamethazine, Sulfadimethoxine, Sulfachloropyridazine Carrier, Metamethoxine, Sulfaquine Oxaline, sulfadiazine, sulfamethoxypyridazine, and sulfamethoxine were deoxygenated by nitrogen fo...

Embodiment 2

[0030] A seven-in-one detection method for sulfonamides, comprising the following steps:

[0031] S1. Synthesize the molecularly imprinted material of sulfonamide by bulk polymerization: 2 parts of sulfathiazole, 1 part of trimethoprim, 3 parts of sulfaquinoxaline, and 1 part of phthaloyl Sulfathiazole, 3 parts of sulfamethiadiazole, 4 parts of sulfamethazine, 12 parts of sulfamethoxazole, 7 parts of sulfamethazine, 3 parts of sulfamethoxine, 21 parts of sulfachloropyridazine carrier, 2 parts Mix one part of m-methoxine, 7 parts of sulfaquinoxaline, 9 parts of sulfadiazine, 1 part of sulfamethoxypyridazine and 2 parts of sulfamethoxine, and mix the mixed sulfathiazole, trimethoprim, and sulfamethoxine Quinoxaline, Phthalylsulfothiazole, Sulfamethiadiazole, Sulfamethazine, Sulfamethoxazole, Sulfamethazine, Sulfadimethoxine, Sulfachloropyridazine Carrier, Metamethoxine, Sulfaquine Oxaline, sulfadiazine, sulfamethoxypyridazine, and sulfamethoxine were deoxygenated by nitrogen fo...

Embodiment 3

[0036] A seven-in-one detection method for sulfonamides, comprising the following steps:

[0037] S1. Synthesize the molecularly imprinted material of sulfonamide by bulk polymerization: 2 parts of sulfathiazole, 1 part of trimethoprim, 3 parts of sulfaquinoxaline, and 1 part of phthaloyl Sulfathiazole, 3 parts of sulfamethiadiazole, 4 parts of sulfamethazine, 12 parts of sulfamethoxazole, 7 parts of sulfamethazine, 3 parts of sulfamethoxine, 21 parts of sulfachloropyridazine carrier, 2 parts Mix one part of m-methoxine, 7 parts of sulfaquinoxaline, 9 parts of sulfadiazine, 1 part of sulfamethoxypyridazine and 2 parts of sulfamethoxine, and mix the mixed sulfathiazole, trimethoprim, and sulfamethoxine Quinoxaline, Phthalylsulfothiazole, Sulfamethiadiazole, Sulfamethazine, Sulfamethoxazole, Sulfamethazine, Sulfadimethoxine, Sulfachloropyridazine Carrier, Metamethoxine, Sulfaquine Oxaline, sulfadiazine, sulfamethoxypyridazine, and sulfamethoxine were deoxygenated by nitrogen fo...

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PUM

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Abstract

The invention discloses a seven-into-one sulfanilamide detection method which comprises a kit and reagents, wherein the reagents comprise sulfathiazole, trimethoprim, sulfaquinoxaline, phthalylsulfathiazole, sulfamethythiadiazole, sulfamethazine, sulfamethoxazole, sulfamerazine, sulfadimethoxypyrimidine, a sulfachlorpyridazine carrier, m-sulfamethoxydiazine, sulfaquinoxaline, sulfadiazine, sulfamethoxypyridazine and sulfametoxydiazine. According to the seven-into-one sulfanilamide detection method and the kit, the sulfathiazole, the trimethoprim, the sulfaquinoxaline, the phthalylsulfathiazole, the sulfamethythiadiazole, the sulfamethazine, the sulfamethoxazole, the sulfamerazine, the sulfadimethoxypyrimidine, the sulfachlorpyridazine carrier, the m-sulfamethoxydiazine, the sulfaquinoxaline, the sulfadiazine, the sulfamethoxypyridazine and the sulfametoxydiazine in a proportioning part of a weight unit are combined in match in a glass container, and convenience can be brought to seven-into-one sulfanilamide detection.

Description

technical field [0001] The invention relates to the technical field of sulfonamide seven-in-one detection, in particular to a sulfonamide seven-in-one detection method and a kit. Background technique [0002] Sulfonamides are artificially synthesized sulfonamide derivatives, which can inhibit Gram-positive bacteria and some negative bacteria, and can treat a variety of bacterial infections. They are widely used in veterinary clinics to treat various livestock and poultry infected by sensitive bacteria. It can also be used as a feed additive to improve the conversion rate of feed and promote animal growth. There are more than a dozen commonly used SAS. However, these drugs have serious side effects, and their long-term existence in the human body will cause many bacteria to develop drug resistance to sulfa drugs, and they have potential carcinogenicity, so they have attracted great attention at home and abroad. Sulfonamides are artificially synthesized sulfonamide derivative...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/31G01N21/78G01N1/38
CPCG01N21/3103G01N1/38G01N21/78
Inventor 徐静赵春城胡勇蒋韦艳刘金杰吴敏芳朱倩倩
Owner WUXI X RES PROD DESIGN & RES
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