A kind of wearable equipment based on composite phase change material and its preparation method
A technology of composite phase change materials and equipment, applied in heat exchange materials, chemical instruments and methods, clothing, etc., can solve the problems of easy-to-leak organic phase change materials such as thermal conductivity and poor encapsulation, and achieve non-corrosive chemical properties, High latent heat of phase change and stable chemical properties
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Embodiment 1
[0038] (1) Preparation of composite phase change materials
[0039] Take lauric acid and stearic acid with a mass ratio of 60.3:39.7, add them to a beaker with a total mass of 50 g, put them on a magnetic stirrer with heating function, set the heating temperature to 100 °C, and the speed to 1800 r / min. Until it is completely melted, the eutectic mixture of lauric acid and stearic acid is obtained, and then cooled to room temperature to obtain a composite phase change material.
[0040] (2) Measuring the physical parameters of composite phase change materials
[0041] Using differential scanning calorimeter, protective atmosphere: nitrogen; flow rate: 15ml / min; heating rate: 5K / min, test temperature range 20℃~50℃. Draw the DSC curve of the composite phase change material of lauric acid and stearic acid, and analyze the phase change temperature and latent heat of phase change. The obtained results are t 1 = 34.316°C and H 1 = 189.73 kJ / kg.
[0042] (3) preparation of microca...
Embodiment 2
[0050] (1) Synthesis of composite phase change materials
[0051] Take lauric acid and myristic acid with a mass ratio of 58:42, put them into a beaker with a total mass of 50g, put them on a magnetic stirrer with heating function, set the heating temperature to 100°C, and the speed to 1400r / min until Completely melted to obtain the eutectic mixture of lauric acid and myristic acid, and then cooled to room temperature to obtain a composite phase change material.
[0052] (2) Measuring the physical parameters of composite phase change materials
[0053] Using differential scanning calorimeter, protective atmosphere: nitrogen; flow rate: 15ml / min; heating rate: 5K / min, test temperature range 20℃~50℃. Draw the DSC curve of the composite phase change material of lauric acid and myristic acid, and analyze the phase change temperature and latent heat of phase change. The obtained results are t 2 =34.273°C, H 2 = 162.801 kJ / kg.
[0054] (3) preparation of microcapsules
[0055] ...
Embodiment 3
[0062] (1) Synthesis of composite phase change materials
[0063] Take lauric acid and palmitic acid with a mass ratio of 69:31, add them to a beaker with a total mass of 50 g, put them on a magnetic stirrer with heating function, set the heating temperature at 100 ° C, and rotate at 1200 r / min until completely melting to obtain a eutectic mixture of lauric acid and palmitic acid, and then cooling to room temperature to obtain a composite phase change material.
[0064] (2) Measuring the physical parameters of composite phase change materials
[0065] Using differential scanning calorimeter, protective atmosphere: nitrogen; flow rate: 15ml / min; heating rate: 5K / min, test temperature range 20℃~50℃. Draw the DSC curve of the composite phase change material of lauric acid and stearic acid, and analyze the phase change temperature and latent heat of phase change. The obtained results are t 3 =33.283°C, H 3 = 166.54 kJ / k.
[0066] (3) preparation of microcapsules
[0067] Firs...
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