Compound composition containing organophosphorus insecticide and chitin synthesized inhibitor and application of compound composition
A compound composition and insecticide technology, applied in the field of pesticides, can solve problems such as difficult effects, achieve good control effects, improve control effects, and improve control effects
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Embodiment 1
[0032] Example 1 4% phoxim·diflubenzuron microcapsule suspension
[0033] Step 1: phoxim 30g, diflubenzuron 10g, sebacoyl chloride 5.8g, polymethylene polyphenylene diisocyanate 2.2g to form A solution, 4% polyvinyl alcohol 600mL as B solution, diethylenetriamine 2.9g, Solution C was composed of 5.1 g of anhydrous sodium carbonate and 200 mL of deionized water. Put the B solution into the reactor and stir rapidly at 1500r / min, add the A solution to the B solution and immediately add the C solution, stir at 300r / min for 2 hours, and obtain a microcapsule slurry containing 40g of active ingredients.
[0034] Step 2: Adjust the microcapsule slurry to neutrality with 10% acetic acid aqueous solution, add 2.5g of emulsifier NP-10, 12g of xanthan gum, 0.5g of silicone defoamer, add deionized water to 1L, and obtain 4 % phoxim · diflubenzuron microcapsule suspension.
Embodiment 2
[0035] Example 2 4% phoxim·diflubenzuron microcapsules
[0036] The method of preparing microcapsules in this example is substantially the same as that in Example 1, the difference is that in step 2, the microcapsule slurry is adjusted to neutrality with 10% acetic acid aqueous solution, and 2 g of lubricating oil and 10 g of lignin sulfonate are added. Sodium phosphate, 8g bentonite, add clay to supplement to 1000g, and obtain 4% phoxim·diflubenzuron microcapsules by extrusion granulator.
Embodiment 3
[0037] Example 3 1% phoxim·chlorfluazuron microcapsule suspension
[0038]Step 1: phoxim 5g, chlorfluazuron 1g, polymethylene polyphenylene diisocyanate 0.8g, xylene 3mL to form A solution, 1% polyvinyl alcohol 40mL, ethylenediamine 0.5g and dodecanebenzenesulfonic acid 1g of sodium is used to form solution B, add solution B to solution A, stir in a high-shear emulsification tank at 2800r / min for 30 minutes, reduce the speed to 300r / min, heat up and encapsulate for 2 hours, and obtain a microcapsule slurry containing 6g of active ingredients .
[0039] Step 2: Adjust the microcapsule slurry to neutrality with 10% acetic acid aqueous solution, add 12g Nongru 500#, 10g dispersant D425 and 20mL ethylene glycol, add deionized water to make up to 600mL to prepare 1% phoxim fluoride pyridineurea microcapsule suspension.
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