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A method for resource utilization of macroalgae hydrothermal carbonization fluid

A technology of hydrothermal carbonization and resource utilization, applied in chemical instruments and methods, climate change adaptation, solid waste removal, etc., can solve the problem of low efficiency of resource utilization in the liquid phase, so as to increase hydrothermal carbon production and promote transformation Effect

Inactive Publication Date: 2021-07-16
DALIAN UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0005] The purpose of the present invention is to provide an economical and efficient resource utilization method for the hydrothermal carbonization of large seaweeds, aiming at the technical bottle diameter with low efficiency of resource utilization of the liquid phase in the hydrothermal carbonization of large seaweeds

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  • A method for resource utilization of macroalgae hydrothermal carbonization fluid

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Effect test

Embodiment 1

[0023] (1) Hydrothermal carbonization

[0024] Collect waste kelp along the coast, wash it with water to remove impurities such as sediment, dry it naturally, and use it as a raw material for hydrothermal carbonization after being crushed; adjust the ratio of raw material to water to 1:20, put this mixture into a hydrothermal reactor, and control The reaction temperature is 220°C, the reaction time is 2 hours, and the seaweed-based hydrothermal carbonization product is obtained; the seaweed-based hydrothermal carbonization product obtained above is subjected to solid-liquid separation, and the hydrothermal charcoal is recovered, and the liquid phase product is collected as the next round of hydrothermal carbonization. Carbonized liquid phase; the liquid phase after 10 rounds of hydrothermal carbonization cycle is the hydrothermal carbonization liquid;

[0025] (2) Hydrothermal charcoal enhanced hydrothermal carbonization liquid methane fermentation

[0026] Add the hydrotherm...

Embodiment 2

[0030] (1) Hydrothermal carbonization

[0031] Collect algae residue after polysaccharide extraction from kelp, wash with water to remove impurities such as sediment, dry naturally, and use it as raw material for hydrothermal carbonization after being crushed; adjust the ratio of raw material to water to 1:15, and put this mixture into hydrothermal reaction In the reactor, the reaction temperature is controlled at 210°C, and the reaction time is 2.5 hours to obtain the seaweed-based hydrothermal carbonization product; after the above-mentioned seaweed-based hydrothermal carbonization product is separated from the solid and liquid, the hydrothermal charcoal is recovered, and the liquid phase product is collected as The liquid phase of the next round of hydrothermal carbonization; the liquid phase after 9 cycles of hydrothermal carbonization is the hydrothermal carbonization liquid;

[0032] (2) Hydrothermal charcoal enhanced hydrothermal carbonization liquid methane fermentatio...

Embodiment 3

[0037] (1) Hydrothermal carbonization

[0038] Collect waste kelp along the coast, wash it with water to remove impurities such as sediment, dry it naturally, and use it as a raw material for hydrothermal carbonization after being crushed; adjust the ratio of raw material to water to 1:20, put this mixture into a hydrothermal reactor, and control The reaction temperature is 230°C, the reaction time is 1.5h, and the seaweed-based hydrothermal carbonization product is obtained; the seaweed-based hydrothermal carbonization product obtained above is subjected to solid-liquid separation, and the hydrothermal charcoal is recovered, and the liquid phase product is collected as the next round of water The liquid phase of thermal carbonization; the liquid phase after 10 cycles of hydrothermal carbonization is the hydrothermal carbonization liquid;

[0039] (2) Hydrothermal charcoal enhanced hydrothermal carbonization liquid methane fermentation

[0040] Add the hydrothermal charcoal and...

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Abstract

The invention provides a method for resource utilization of large seaweed hydrothermal carbonization fluid, and belongs to the technical field of environmental engineering solid waste resource recovery. In the process of hydrothermal carbonization of large seaweed, the hydrothermal carbonization liquid is recycled. While increasing the production of hydrothermal charcoal, it can strengthen the thermochemical transformation of inhibitory organic matter. Thermal charcoal remediation of coastal polluted soil. The effect and benefit of the present invention are that the complete resource utilization of hydrothermal carbonization products of large algae can be realized, and the technical bottle diameter of low methane production efficiency and methane purity during conventional anaerobic digestion treatment of hydrothermal carbonization liquid can be effectively overcome, and the produced high-purity Both methane and hydrothermal charcoal can be used to heat the hydrothermal reactor to achieve energy self-sufficiency, and have broad application prospects in the resource utilization of seaweed waste and the restoration of coastal soil and wetland pollution.

Description

technical field [0001] The invention belongs to the technical field of environmental engineering solid waste resource utilization, and relates to a method for resource utilization of large seaweed hydrothermal carbonization fluid. Background technique [0002] Offshore farming of macroalgae plays an important role in the marine ecosystem, which can increase the ocean's ability to absorb carbon dioxide and reduce the impact of carbon dioxide on the global warming effect. At the same time, large seaweed can absorb a large amount of organic matter, nitrogen, phosphorus, etc. in the water body, improve the material circulation capacity, and improve the eutrophication of the sea area. It is an effective restoration strategy for the coastal ecological environment. However, if not handled properly, macroalgae can naturally decline in large numbers in the ocean, causing a series of environmental problems. In addition, in the process of preparing high value-added products from macro...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B09B3/00B09B5/00B09C1/10C10B53/02C10B57/00C02F11/04
CPCB09B5/00B09C1/10C10B53/02C10B57/00C02F11/04B09B3/80Y02A40/22Y02E50/10Y02E50/30
Inventor 王竞王奉博吴昊
Owner DALIAN UNIV OF TECH