Method for detecting magnetic substances of lithium ion battery material
A technology of lithium-ion batteries and magnetic substances, which is applied in measuring devices, particle size analysis, scientific instruments, etc., can solve the problems that the polymer wear-resistant layer cannot be removed, and the magnetic substances are difficult to collect.
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Embodiment 1
[0034] 1. Take 300g of graphene slurry in a 1L container, add 300g of primary water to adjust the viscosity of the solution to be tested to 3000 Pascal seconds;
[0035] 2. Put the polytetrafluoroethylene insulating layer on the magnetic rod, and the magnetic flux of the magnetic rod is 12000 gauss; stir the magnetic rod covered with the polytetrafluoroethylene insulating layer at 30 rpm / min for 30 minutes to make the magnetic rod Thoroughly extract the magnetic substances in the solution to be tested;
[0036] 3. Put the extracted magnetic rod covered with polytetrafluoroethylene isolation layer into a container filled with first-grade water, stir to clean the magnetic rod; wash 5 times until the first-grade water is clear; finally put the polytetrafluoroethylene The isolation layer is removed from the magnetic rod, and the magnetic substance is transferred to clean first-class water to obtain the dispersion to be tested;
[0037] 4. Pass the dispersion to be tested through ...
Embodiment 2
[0042] 1. Take 300g of carbon nanotube slurry in a 1L container, add 300g of nitrogen methylpyrrolidone to adjust the viscosity to 3500 Pascal s for the solution to be tested;
[0043] 2. Put the polytetrafluoroethylene insulating layer on the magnetic rod, and the magnetic flux of the magnetic rod is 12000 gauss; stir the magnetic rod covered with the polytetrafluoroethylene insulating layer at 30 rpm / min for 30 minutes to make the magnetic rod Thoroughly extract the magnetic substances in the solution to be tested;
[0044] 3. Put the extracted magnetic rod covered with polytetrafluoroethylene isolation layer into the container containing nitrogen methyl pyrrolidone, stir and clean the magnetic rod with ultrasound (30kHz); wash 6 times until the nitrogen methyl pyrrolidone Pyrrolidone is clarified; finally, the polytetrafluoroethylene insulating layer is removed from the magnetic rod, and the magnetic substance is transferred to clean nitrogen methyl pyrrolidone to obtain th...
Embodiment 3
[0049] 1. Take 300g of graphene composite slurry in a 1L container,
[0050] Add 300g nitrogen methyl pyrrolidone to adjust the viscosity to be the solution to be tested at 3200 Pascal seconds;
[0051] 2. Put the polytetrafluoroethylene isolation layer on the magnetic rod, and the magnetic flux of the magnetic rod is 12000 gauss;
[0052] Stir the solution to be tested with a magnetic rod covered with a polytetrafluoroethylene isolation layer at 45 rpm / min for 45 minutes, so that the magnetic rod can completely extract the magnetic substance in the solution to be tested;
[0053] 3. Put the extracted magnetic rod covered with polytetrafluoroethylene isolation layer into the container containing nitrogen methyl pyrrolidone, stir and clean the magnetic rod with ultrasound (30kHz); wash 6 times until the nitrogen methyl pyrrolidone Pyrrolidone is clarified; finally, the polytetrafluoroethylene insulating layer is removed from the magnetic rod, and the magnetic substance is tran...
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