Polarizing plate and image display device comprising same
A polarizer and polarizer technology, applied in the field of polarizers, can solve the problems of image display device visibility deterioration, in-plane phase difference, refractive index difference, etc.
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Synthetic example 1
[0092] Synthesis Example 1: Synthesis of Polymodified Urethane Acrylate
[0093] As a polyvalent isocyanate-based compound having three or more functional groups, HDI-based trimer DN980S manufactured by Aekyung Chemical Co., Ltd. was used; as polyethylene glycol-modified (meth)acrylate For the class of compounds, polyethylene glycol monoacrylate (Mn=300) and polyethylene glycol monoacrylate (Mn=500) having different numbers of polyethylene glycol repeating units and thus different number average molecular weights were used, respectively.
[0094] 40 g of polyvalent isocyanate-based compounds, 30 g of polyethylene glycol monoacrylate (Mn=300) and 30 g of polyethylene glycol monoacrylate (Mn=500) were mixed with 0.1 g of DBTDL (dibutyltin dilaurate) and 200 g of formazan Ethyl ketone was mixed, and the mixture was stirred at 60° C. for 5 hours to perform a carbamate reaction. By completing the urethane reaction, the polyethylene glycol-modified polyfunctional urethane (meth)acr...
Synthetic example 2
[0096] Synthesis Example 2: Synthesis of High Molecular Weight Copolymer
[0097] A high molecular weight copolymer (PMMA-PBA block copolymer) was prepared by reversible addition-fragmentation chain transfer polymerization (RAFT polymerization) of polymethyl methacrylate (PMMA) and poly(butyl acrylate) (PBA). Herein, the volume ratio of PMMA to PBA is about 1:1, and the number average molecular weight is about 30000 g / mol. In addition, the average particle diameter of the micellar structure formed by the self-assembly of the PMMA-PBA block copolymer was about 15 nm.
preparation example 1
[0098] Preparation Example 1: Preparation of Coating Solution (A) for Forming the First Hard Coat
[0099] The polymodified urethane acrylate prepared in 38.74g trimethylpropyl triacrylate (TMPTA), 30.99g synthetic example 1, the high molecular weight copolymer prepared in 7.75g synthetic example 2, 2.31g TPO (with Initiator for photocuring, manufactured by Ciba Company), 0.21 g of T270 (leveling agent manufactured by Tego Inc.), and solvent 13.33 g of ethyl methyl ketone (MEK) and 6.67 g of methyl isobutyl ketone were mixed to A coating solution (A) for forming the first hard coat layer was prepared.
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