Burning rate modifier for carbon-based zinc oxide composite propellant and low-temperature preparation method thereof

A carbon-based zinc oxide and propellant technology, applied in the direction of offensive equipment, gaseous chemical plating, ammonium perchlorate composition, etc., to achieve the effects of excellent burning rate adjustment performance, optimized energy release structure, and excellent burning rate adjustment ability

Active Publication Date: 2021-11-23
XIAN MODERN CHEM RES INST
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] The present invention proposes a burning rate regulator for carbon-based zinc oxide composite propellant and its low-temperature preparation method to solve the technical problem of how to prepare the burning rate regulator for carbon-based zinc oxide composite propellant

Method used

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  • Burning rate modifier for carbon-based zinc oxide composite propellant and low-temperature preparation method thereof
  • Burning rate modifier for carbon-based zinc oxide composite propellant and low-temperature preparation method thereof
  • Burning rate modifier for carbon-based zinc oxide composite propellant and low-temperature preparation method thereof

Examples

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Embodiment 1

[0037] This example proposes a combustor modifier and a low temperature preparation method for a carbon-based zinc oxide composite propellant, and the carbon-based substrate material used is an activated carbon (AC) material, a specific surface area of ​​1250 square meters / gram, and the preparation method specifically includes the following steps. :

[0038] Step 1, such as figure 1 As shown, the activated carbon is applied to the porous container and then placed in the reaction chamber of the chemical vapor deposition apparatus, and the quartz crystal microfales are attached to the sample outlet of the chemical reactant deposition equipment, and then the chemical reaction deposition equipment is entered and export;

[0039] Step 2, heat the chemical vapor deposition reaction chamber by electrically heating wire, so that the temperature is at 100 ° C;

[0040] Step 3, the flow rate of 100 sccm is introduced into the reaction chamber from the inlet of the vapor deposition equipme...

Embodiment 2

[0051] In this example, a combustor-based zinc oxide composite propellant was proposed for a combustor modifier and a low temperature preparation method. The carbon-based substrate used was carbon nanotube (CNT) material, a specific surface area of ​​820 square meters / gram, and the preparation method specific The following steps:

[0052] Step 1, laid the carbon nanotube after the sample tank is placed in the reaction chamber of the chemical vapor deposition apparatus, and then the chemical reaction deposition equipment is entered and export;

[0053] Step 2, heat the chemical vapor deposition chamber by electrically heating wire, so that the temperature is at 80 ° C;

[0054] Step 3, the nitrogen of the flow rate 50sccm is passed from the inlet of the vapor deposition equipment to the reaction chamber, and the vacuum pump is taken with a vacuum pump at the outlet of the vapor deposition apparatus, so that the vacuum in the reaction chamber is around 30 Pa;

[0055] Step 4, open...

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Abstract

The present invention proposes a low-temperature preparation method of a burning rate regulator for carbon-based zinc oxide composite propellants. The preparation method mainly includes exposing the carbon-based substrate to diethyl zinc vapor, so that the vapor molecules are adsorbed on the surface of the carbon-based substrate; Use an inert gas to blow the physically adsorbed diethyl zinc molecules on the surface of the substrate away from its surface; expose the carbon-based substrate to water vapor, so that the water vapor molecules react chemically with the adsorbed diethyl zinc molecules; use The inert gas blows by-products and excess vapor molecules off the surface of the substrate. Compared with traditional burning rate regulators and carbon-based burning rate regulators prepared by other methods, the burning rate regulator prepared by the present invention has excellent burning rate regulation ability, can effectively reduce the decomposition temperature of AP, optimize the energy release structure, and the preparation temperature Gentle, high degree of automation, good safety performance, the product can be used directly without post-processing, easy to achieve mass production, and environmentally friendly.

Description

Technical field [0001] The present invention belongs to the surface modification of the powder material and the art of preparation thereof, and is, according to the field of preparation. Background technique [0002] The combustion performance of the propellant has an important impact on the ballistic performance of the rocket engine. The high and low of the fuel determines the working length and flight speed of the rocket engine, and the size of the combustion rate is affected by the external conditions (temperature and pressure) directly affects the stability of engine operating performance. Therefore, the combustion performance of control and regulating rocket propellants is important to meet the performance needs of various artillery, rocket engines, and rocket weapons. The fuel regulator is the most commonly used method for adjusting and improving the combustion performance of the propellant. Conventional combustion regulators can be controllable adjusted to the combustion a...

Claims

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Application Information

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Patent Type & AuthorityPatents(China)
IPC IPC(8): C06B23/00C06B29/22C06D5/06C23C16/40C23C16/455
CPCC06B23/007C06B29/22C06D5/06C23C16/407C23C16/4417C23C16/45527
Inventor冯昊李建国龚婷张王乐惠龙飞秦利军李丹
OwnerXIAN MODERN CHEM RES INST