A kind of intelligent light-emitting switch material with self-encryption function, preparation method and application thereof
A switching material, self-encryption technology, applied in luminescent materials, computer material science, chemical instruments and methods, etc., can solve the problems of limited application prospects of encryption-decryption technology, non-reusable, and inability to erase information, and achieve good repeatability. The effect of usability, easy storage, and high safety
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[0018] The specific implementation manners of the present invention will be further described below in conjunction with the accompanying drawings and technical solutions.
[0019] Step 1: Preparation of Pt(II) smart light-emitting switch complex with self-encryption function.
[0020] [4,4'-bis(trimethylsilylethynyl)-2,2'-bipyridyl]platinum dichloride intermediate and 2.5 equivalents of 3-bromophenylacetylene, 0.001-0.10 equivalents of cuprous iodide, sequentially Add it into anhydrous diisopropylamine and dichloromethane (volume ratio 1:10) solution, and stir at room temperature under nitrogen protection for 24 hours. After the reaction was completed, the solvent was distilled off under reduced pressure, and then separated and purified by column chromatography to obtain the product with a yield of 83%. Elemental analysis results: press C 36 h 32 Br 2 N 2 PtSi 2 Calculated (%) C 47.85, H 3.57, N 3.10; found (%) C 47.88, H 3.61, N 3.05. 1 H NMR (500MHz, DMSO, ppm): 9.447...
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