Low-smoke halogen-free flame-retardant cable and preparation method thereof
A flame-retardant cable and sheath technology, which is applied in the direction of cable/conductor manufacturing, insulated cables, cables, etc., can solve the problems of low biodegradation rate of halogen compounds, large amount of production, environmental pollution, etc.
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preparation example 1
[0080] A kind of microencapsulation red phosphorus, is made by following method:
[0081] Step 1: Put 1 kg of red phosphorus in 1 kg of water, add sodium bicarbonate solution while stirring to make the mixed solution neutral, and obtain pretreated red phosphorus after drying;
[0082] Step 2: Add the pretreated red phosphorus obtained in step 1 into 0.8 kg of zinc sulfate and calcium sulfate mixed solution, wherein the weight ratio of zinc sulfate to calcium sulfate is 1:2, add sodium hydroxide solution to the mixed solution, The pH value of the mixed solution is 8, and the inorganic coated red phosphorus is obtained after drying;
[0083] Step 3: After soaking the inorganic coated red phosphorus obtained in step 2 in water for 2 days, add 10 g of sodium lauryl sulfate to the water soaked with red phosphorus, stir for 5 minutes, add saturated urea solution, and the weight of urea is 20 g, and continue stirring After 10 minutes, add formaldehyde solution dropwise. The weight o...
preparation example 2
[0085] A kind of microencapsulation red phosphorus, is made by following method:
[0086] Step 1: Put 1 kg of red phosphorus in 1 kg of water, add sodium bicarbonate solution while stirring to make the mixed solution neutral, and obtain pretreated red phosphorus after drying;
[0087] Step 2: Add the pretreated red phosphorus obtained in step 1 into 0.8 kg of zinc sulfate and calcium sulfate mixed solution, wherein the weight ratio of zinc sulfate to calcium sulfate is 1:1, add sodium hydroxide solution to the mixed solution, The pH value of the mixed solution is 9, and the inorganic coated red phosphorus is obtained after drying;
[0088] Step 3: After soaking the inorganic coated red phosphorus obtained in step 2 in water for 1 day, add 20 g of sodium lauryl sulfate to the water soaked with red phosphorus, stir for 10 minutes, add saturated urea solution, and the weight of urea is 50 g, and continue stirring After 5 minutes, add formaldehyde solution dropwise. The weight of...
preparation example 3
[0090] A kind of microencapsulation red phosphorus, is made by following method:
[0091] Step 1: Put 1 kg of red phosphorus in 1 kg of water, add sodium bicarbonate solution while stirring to make the mixed solution neutral, and obtain pretreated red phosphorus after drying;
[0092] Step 2: Add the pretreated red phosphorus obtained in step 1 into 0.8kg of zinc sulfate and calcium sulfate mixed solution, wherein the weight ratio of zinc sulfate to calcium sulfate is 1:1.5, add sodium hydroxide solution to the mixed solution, The pH value of the mixed solution is 8.5, and the inorganic coated red phosphorus is obtained after drying;
[0093] Step 3: After soaking the inorganic coated red phosphorus obtained in step 2 in water for 1.5d, add 15g of sodium lauryl sulfate to the water soaked with red phosphorus, stir for 8min, add urea saturated solution, and the weight of urea is 35g, continue Stir for 8 minutes, and then add formaldehyde solution dropwise. The weight of formal...
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