Method for determining gallium content in antibacterial stainless steel
A technology of antibacterial stainless steel and gallium content, applied in material excitation analysis, thermal excitation analysis, etc., can solve problems such as blanks, and achieve the effect of good accuracy, good reproducibility and simple operation
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[0034] In the present embodiment, the assay method of gallium content in 304 antibacterial stainless steels is as follows:
[0035] (1) Measured on an inductively coupled plasma atomic emission spectrometer (Optima7300DV, Perkin Elemer, USA), the optimized working conditions of the instrument are as follows: the high-frequency generator power is 1.2kW; the plasma gas flow rate is 16mL / min; The air flow rate is 1.0mL / min; the auxiliary air flow rate is 0.2mL / min; the solution lifting volume is 1.5mL / min; the integration time is 2-5s; the observation direction is axial; the observation height is 11mm;
[0036] (2) Reagents:
[0037] (2.1) Gallium single element standard solution (1000 μg / mL, National Iron and Steel Materials Testing Center Iron and Steel Research Institute);
[0038] (2.2) Iron single element standard solution (10mg / mL): prepared by dissolving metallic iron with a purity of not less than 99.99wt% in hydrochloric acid and nitric acid;
[0039] (2.3) Hydrochlori...
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