Dry adhesives
a technology of adhesives and adhesives, applied in the field of dry adhesives, can solve the problems of ink soluble, complicated branched structure of gecko's setae, and image printing with such inks may not be waterfas
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examples 1 to 5
Micro-Featured and Nano-Featured Surfaces
[0284]The surface of aluminum sheets of a thickness of about 0.30 mm were treated according to process 200 as described above using various conditions. These different process conditions are shown in Table III below.
TABLE IIIProcessingEXAMPLESStepsConditions12345DegreasingNaOH and sodiumYesYesYesYesYesgluconateMechanicalNylon brush & pumiceNoNoYesNoYesGrainingstone powderElectrolyticHCl (6.00 g / L)1,000GrainingHCl (8.00 g / L) &1,250270276(C / dm2)CH3COOH (16.0 g / L)HNO3 (10 g / L)160AnodizationH2SO4 (140 g / L)5.605.605.605.60(A / dm2)H3PO4 (160 g / L)7.00FunctionalizationNaH2PO4 (50.0 g / L) &YesYesYesNaF (0.80 g / L)Vinyl phosphoric andYesacrylic copolymer(0.30 g / L)Oxide weight2.701.802.702.20(g / m2)Ra (μm)0.650.520.270.420.60RSm (nm)242622044200
[0285]In Example 1, the surface of the aluminum sheet was pre-treated by degreasing, micro-featured by electrolytic graining in a 6.0 g / L HCl solution with 1,000 C / dm2 of alternating current density, nano-featured by...
example 6
Micro-Featured and Nano-Featured Surface
[0290]A biaxially oriented polyethylene terephthalate film (PET) having a thickness of 30 μm and containing 30° A Zeolite A (mean particle size 1.0 μm) and 5% calcium carbonate (mean particle size 2.0 μm) was extruded 260° C. from a twin screw extruder. It was then stretched to a 3:1 ratio at 130° C. The stretched film was then dipped in a 2M hydrochloric acid solution at 40° C. for 24 hours to partially dissolve the calcium carbonate, which created micropores on the surface. The treated film was then washed with water and dried in a hot air oven at 110° C. It was then dipped in an aqueous polymeric solution containing 5% of silica colloid particles (Ludox HS40 and Ludox SK, available from Dupont, USA), and then dried in a hot air oven at 120° C. This created nanopores on the surface. For this surface, the Ra is about 0.50 μm and RSm is 400 nm. FIG. 5 shows a scanning electron micrograph of the treated PET film.
Observations Concerning Examples...
example 7
Self-Adhesive
[0301]An anodized aluminum sheet (size 20 cm×30 cm, thickness of 0.15 mm) comprising micro-features and nano-features (Ra 0.25 μm and RSm 26 nm) was provided in accordance with the above. The sheet was dipped into an ethanol solution containing 5 g / L of triethoxysilane and a trace of hydrochloric acid at room temperature. The sheet was then dried in a hot air oven at 80° C. for 3 minutes. A heat curable silicone elastomer composition (QLE1031, available from Quantum Silicones, Virginia, USA) was screen printed on the treated aluminum sheet to form a pattern of round dots having a diameter about 2.0 mm. The spacing between the round dots was about 4.0 mm. The sheet was then cured at 150° C. for 20 minutes in a hot air oven to produce surface tack-free silicone compliant dots having a thickness of about 30 μm and which strongly adhered to the porous aluminum sheet. The hardness of the silicone compliant dots was measured and was found to be about 25 Shore-A.
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