Ligand
a technology of ligands and ligands, applied in the field of ligands, can solve the problems of inability to control the ratio of binding sites to each antigen or epitope in the assembled molecule, inability to control the ratio of binding sites to each antigen or epitope, and inability to combine variable domains. to achieve the effect of increasing the half-life of ligands
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example 1
Selection of a Dual Specific scFv Antibody (K8) Directed Against Human Serum Albumin (HSA) and β-Galactosidase (β-Gal)
[0491]This example explains a method for making a dual specific antibody directed against β-gal and HSA in which a repertoire of Vκ variable domains linked to a germ line (dummy) VH domain is selected for binding to 3-gal and a repertoire of VH variable domains linked to a -germ line (dummy) Vκ domain is selected for binding to HSA. The selected variable VH HSA and Vκ β-gal domains are then combined and the antibodies selected for binding to β-gal and HSA. HSA is a half-life increasing protein found in human blood.
[0492]Four human phage antibody libraries were used in this experiment.
Library 1-Germ line Vκ / DVT VH8.46 × 107Library 2-Germ line Vκ / NNK VH9.64 × 107Library 3-Germ line VH / DVT Vκ1.47 × 108Library 4-Germ line VH / NNK Vκ1.45 × 108
[0493]All libraries are based on a single human framework for VH (V3-23 / DP47 and JH4b) and Vκ (O12 / O2 / DPK9 and Jκ1) with side chain ...
example 2
Characterisation of the Binding Properties of the K8 Antibody
[0499]Firstly, the binding properties of the K8 antibody were characterised by the monoclonal phage ELISA. A 96-well plate was coated with 100 μl of HSA and β-gal alongside with alkaline phosphatase (APS), bovine serum albumin (BSA), peanut agglutinin, lysozyme and cytochrome c (to check for cross-reactivity) at 10 μg / ml concentration in PBS overnight at 4° C. The phagemid from K8 clone was rescued with KM13 as described by Harrison et al., (1996) and the supernatant (50 μl) containing phage assayed directly. A standard ELISA protocol was followed (Hoogenboom et al., 1991) using detection of bound phage with anti-M13-HRP conjugate. The dual specific K8 antibody was found to bind to HSA and β-gal when displayed on the surface of the phage with absorbance signals greater than 1.0 (FIG. 4). Strong binding to BSA was also observed (FIG. 4). Since HSA and BSA are 76% homologous on the amino acid level, it is not surprising that...
example 4
Creation and Characterisation of the Dual Specific ScFv Antibodies (VH1 / VH2 Directed Against Antigens A and B and VK1 / VK2 Directed Against Antigens C and D)
[0506]This example demonstrates that dual specific ScFv antibodies (VH1 / VH2 directed against antigens A and B and VK1 / VK2 directed against antigens C and D) could be created by combining Vκ and VH single domains selected against respective antigens in a ScFv vector.
[0507]To create dual specific antibody VH1 / VH2, VH1 single domain is excised from variable domain vector 1 (FIG. 7) by NcoI / XhoI digestion and ligated into NcoI / XhoI digested variable domain vector 2 (FIG. 7) to create VH1 / variable domain vector 2. VH2 single domain is PCR amplified from variable domain vector 1 using primers to introduce SalI restriction site to the 5′ end and Nod restriction site to the 3′ end. The PCR product is then digested with SalI / NotI and ligated into SalI / NotI digested VH1 / variable domain vector 2 to create VH1 / VH2 / variable domain vector 2.
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