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Silicone composite particles, making method, and cosmetic composition

a technology of composite particles and silicone, applied in the field of silicone composite particles, can solve the problems of uv radiation transmission, conventional uv screening cosmetic composition loses its uv screening effect, etc., and achieve the effect of pleasing us

Active Publication Date: 2016-02-23
SHIN ETSU CHEM IND CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

[0030]The silicone composite particles may be compounded in a cosmetic composition to exert a UV screening effect or bactericidal property inherent to inorganic nano-particles and to impart a pleasant feel on use inherent to silicone. The method is effective for preparing the silicone composite particles. A cosmetic composition comprising the silicone composite particles has many advantages.

Problems solved by technology

A UV screening cosmetic composition having conventional silicone composite particles compounded therein has the problem that since the silicone composite particles have a large particle size, UV radiation is transmitted by the silicone composite particles unless a substance having a UV screening effect such as titanium oxide is incorporated in the silicone composite particles.
Thus the conventional UV screening cosmetic composition loses its UV screening effect.

Method used

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  • Silicone composite particles, making method, and cosmetic composition
  • Silicone composite particles, making method, and cosmetic composition

Examples

Experimental program
Comparison scheme
Effect test

example 1

Titanium Oxide-Laden Silicone Resin-Coated Silicone Elastomer Composite Particles

[0126]A glass beaker having a volume of 1 liter was charged with 50 g of methylvinylpolysiloxane of formula (1) having a viscosity of 580 mm2 / s and 19 g of methylhydrogenpolysiloxane of formula (2) having a viscosity of 30 mm2 / s (to give 1.06 hydrosilyl groups per olefinic unsaturated group). Using a homomixer, the ingredients were agitated at 2,000 rpm and dissolved. Then 3 g of polyoxyethylene lauryl ether (molar amount of ethylene oxide added=9 moles) and 55 g of water were added. Using a homomixer, the ingredients were agitated at 6,000 rpm whereupon an oil-in-water type emulsion was formed and a viscosity buildup was observed. Agitation was continued for a further 15 minutes. While agitating at 2,000 rpm, 421 g of water was added to the emulsion which turned into a uniform white emulsion. The emulsion was transferred into a 1-liter glass flask equipped with an agitator having an anchor shaped impel...

example 2

Iron Oxide-Laden Silicone Resin-Coated Silicone Elastomer Composite Particles

[0132]As in Example 1, a water dispersion of silicone elastomer spherical particles was prepared. 867 g of the water dispersion of silicone elastomer spherical particles was transferred into a 3-liter glass flask equipped with an agitator having an anchor shaped impeller, to which were added 33 g of a water dispersion of iron oxide nano-particles (trade name, JC-FH04, by JFE Chemical Co., Ltd., average particle size 70 nm) (to give 7.3 parts of iron oxide per 100 parts of silicone elastomer spherical particles), 10 g of 30 wt % dodecyltrimethylammonium chloride aqueous solution, 1,975 g of water and 57 g of 28 wt % ammonia water. At this point, the liquid was at pH 11.2. After it was conditioned at 5-10° C., 58 g of methyltrimethoxysilane (to give 6.3 parts of polyorganosilsesquioxane per 100 parts of silicone elastomer spherical particles after hydrolytic condensation reaction) was added dropwise over 20 m...

example 3

Zinc Oxide-Laden Silicone Resin-Coated Silicone Elastomer Composite Particles

[0135]As in Example 1, a water dispersion of silicone elastomer spherical particles was prepared. 867 g of the water dispersion of silicone elastomer spherical particles was transferred into a 3-liter glass flask equipped with an agitator having an anchor shaped impeller, to which were added 51 g of a water dispersion of zinc oxide nano-particles (trade name, ZW-143, by Sumitomo Osaka Cement Co., Ltd., zinc oxide concentration 30 wt %, average particle size 20 nm) (to give 3.4 parts of zinc oxide per 100 parts of silicone elastomer spherical particles), 1,967 g of water and 57 g of 28 wt % ammonia water. At this point, the liquid was at pH 11.3. After it was conditioned at 5-10° C., a mixture of 58 g of methyltrimethoxysilane and 2 g of γ-aminopropyltrimethoxysilane (to give 6.4 parts of polyorganosilsesquioxane per 100 parts of silicone elastomer spherical particles after hydrolytic condensation reaction) ...

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Abstract

Silicone composite particles are provided in which silicone elastomer spherical particles having a volume average particle size of 0.1-100 μm are coated with an organosilsesquioxane-based silicone resin containing inorganic nano-particles having a volume average particle size of up to 100 nm. The silicone composite particles are compounded in a cosmetic composition to exert a UV screening effect or bactericidal property inherent to inorganic nano-particles and to impart a pleasant feel on use. A preparing method and a cosmetic composition are also provided.

Description

CROSS-REFERENCE TO RELATED APPLICATION[0001]This non-provisional application claims priority under 35 U.S.C. §119(a) on Patent Application No. 2009-257867 filed in Japan on Nov. 11, 2009, the entire contents of which are hereby incorporated by reference.TECHNICAL FIELD[0002]This invention relates to silicone composite particles, a method for preparing the same, and a cosmetic composition comprising the same.BACKGROUND ART[0003]From the past, silicone particles are often used in cosmetic compositions for the purposes of imparting a pleasant feel on use (e.g., smooth or silky feel) and spreadability thereto. In particular, fine particles comprising spherical fine particles of silicone elastomer coated with polyorganosilsesquioxane as disclosed in JP-A H07-196815 are used in many cosmetic compositions because of soft feel, non-cohesion, and good dispersion.[0004]The silicone particles do not possess a UV screen effect. When these particles are compounded in cosmetic compositions intend...

Claims

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Application Information

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Patent Type & Authority Patents(United States)
IPC IPC(8): A61K8/58A61Q17/04C08J3/12A61K8/891A61Q15/00A61Q17/00A61K8/29A61K8/27A61K8/19C08L83/04C08G77/12C08G77/20
CPCC08L83/04A61K8/19A61K8/27A61K8/29A61K8/891A61Q15/00A61Q17/005A61Q17/04C08J3/12C08J3/128C08L83/00A61K2800/412A61K2800/413C08G77/12C08G77/20C08J2383/04
Inventor INOKUCHI, YOSHINORIINABA, RYUICHI
Owner SHIN ETSU CHEM IND CO LTD
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