Process for separating methylisobutanone synthesized from acetone
A technology for the separation of methyl isobutyl ketone and its separation method, which is applied in the separation field of synthesizing methyl isobutyl ketone from acetone, can solve the problems of high consumption of raw material acetone, achieve the effects of improving competitiveness, reducing consumption, and reducing production costs
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Embodiment 1
[0036] The flow adopted in the embodiment is the flow introduced in the second scheme.
[0037] 1, the situation of the raw material used in embodiment
[0038] Table 1 is composed of raw materials sent from the reaction system to the separation system.
[0039] Table 1 Raw material composition
[0040] name
Composition, wt%
h 2 o
5.76
2-MPA
0.35
AC
63.04
MIBK
29.00
DAA
0.25
DIBK
1.10
TMB
0.50
[0041] 2. Introduction to the process
[0042] The material coming from the reaction system first enters the 2-methylpentane tower 1,2-methylpentane and acetone are azeotroped, and the 2-methylpentane is steamed from the top of the tower in the form of an azeotrope (column 1 under normal pressure The azeotrope theoretical composition is 56wt% 2-methylpentane and 44wt% acetone; in experimental operation, the azeotrope composition is 25wt% 2-methylpentane and 75wt% acetone)...
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