Melanin extracted from Cinnamomum burmanni peel, preparation method and uses thereof
A technology for melanin and peel, which is applied in chemical instruments and methods, azo dyes, organic dyes, etc., and can solve problems such as no extraction of melanin.
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Embodiment 1
[0020] 1) Get fresh pericarp of Yinxiang fruit, wash it with clear water and dry it for later use; take 100 grams of Yinxiang pericarp, extract it with 2 liters of ammonia water with a volume concentration of 10% at normal temperature for 12 hours, filter it with double-layer gauze, Separating the pericarp of Cinnamomum burmanii and other impurities to obtain the extract;
[0021] 2) Use 2 mol / L hydrochloric acid to adjust the pH value of the extract to 2.5 to precipitate the melanin, separate the melanin precipitate by suction filtration, and then dry the melanin precipitate in a vacuum environment at 50°C for 2 hours to obtain a crude melanin extract thing;
[0022] 3) Put 4 grams of crude melanin extract into 100 ml of 7mol / L hydrochloric acid, hydrolyze in a water bath at 100°C for 6 hours, and then separate the melanin precipitate by suction filtration to obtain melanin;
[0023] 4) Dissolve the obtained melanin with 100 ml of ammonia water with a volume concentration of...
Embodiment 2
[0026] 1) Take the pericarp of 8 minutes ripe yin xiang fruit, wash it with clear water and dry it for later use; take 5 kg of yin xiang fruit peel, extract it with 400 liters of 0.5mol / L sodium hydroxide at normal temperature for 24 hours, and wash it with a double-layer Filtrate with gauze to separate the pericarp of Cinnamomum burmanii and other impurities to obtain the extract;
[0027] 2) Adjust the pH value of the extract to 3 with acetic acid with a volume concentration of 20%, so that the melanin is precipitated, and the melanin precipitate is separated by suction filtration, and then the melanin precipitate is dried at 30°C for 6 hours to obtain the crude melanin Extract;
[0028] 3) put 0.2 kg of crude melanin extract into 10 liters of 4 mol / L hydrochloric acid, hydrolyze in a water bath at 60° C. for 8 hours, and then separate the melanin precipitate by suction filtration to obtain melanin;
[0029] 4) Dissolve the obtained melanin with 2 liters of 1mol / L sodium hy...
Embodiment 3
[0032] 1) Get the pericarp of fresh yin xiang fruit, wash it with clear water and dry it for subsequent use; get 20 kilograms of yin yang fruit peel, use 200 liters of volume concentration to be 20% ammonia water for leaching at normal temperature for 16 hours, filter with double-layer gauze, Separating the pericarp of Cinnamomum burmanii and other impurities to obtain the extract;
[0033] 2) Use 1 mol / L hydrochloric acid to adjust the pH value of the extract to 2.5 to precipitate the melanin, separate the melanin precipitate by suction filtration, and then dry the melanin precipitate in a vacuum environment at 50°C for 5 hours to obtain a crude melanin extract thing;
[0034] 3) Put 1 kg of the crude melanin extract into 12 liters of 4 mol / L hydrochloric acid, hydrolyze it in a water bath at 90°C for 6 hours, and then separate the melanin precipitate by suction filtration to obtain melanin;
[0035] 4) Dissolve the obtained melanin with 30 liters of 0.5mol / L sodium hydroxid...
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