Seepage-proofing thickening agent for textile printing and preparation method thereof
A textile and anti-seepage technology, which is applied in the direction of textiles, papermaking, dyeing, etc., can solve the problems of no public information and poor use effect, and achieve the effect of simple production process, low cost and easy operation control
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Embodiment 1
[0017] (1) Neutralization reaction: Add 161 grams of methacrylic acid and 55 grams of acrylic acid in a stainless steel kettle, neutralize with 332 grams of ammonia water with a concentration of 20% by weight, keep the temperature at 0-40 ° C, and adjust the pH value of the product to 6.5 , then add 18 grams of methacrylamidopropyl dimethylamine and 2.5 grams of glyceryl dimethacrylate into the reaction kettle, stir evenly to obtain neutralizing liquid;
[0018] (2) Emulsification reaction: Add 51 grams of No. 200 solvent oil to the emulsification reaction kettle, add 19 grams of sorbitan monooleate S-80, add the neutralizing solution completely while stirring at a high speed, and finally add water 170g, fully emulsified at 40-50°C for 30 minutes;
[0019] (3) Polymerization reaction: The temperature of the emulsification reaction kettle is raised to 65-68°C, and a mixture of 0.15 grams of initiator sodium persulfate and 50 grams of water is added dropwise to make it polymeriz...
Embodiment 2
[0021] The weight ratio of raw materials is: 169 grams of methacrylic acid, 59 grams of acrylic acid, 352 grams of ammonia water with a concentration of 20% by weight, 21 grams of methacrylamide propyl dimethylamine, and 3.4 grams of glycerol dimethacrylate. Take 22 grams of Sorbitan Monooleate S-80, 59 grams of No. 200 solvent oil, a mixture of 0.16 grams of sodium persulfate and 50 grams of water, fatty alcohol polyoxyethylene ether AEO 9 Get 4 grams, 198 grams of water, the technological process of production is with embodiment 1.
Embodiment 3
[0023] The weight ratio of raw materials is: 165 grams of methacrylic acid, 57 grams of acrylic acid, 342 grams of ammonia water with a concentration of 20% by weight, 20 grams of methacrylamide propyl dimethylamine, 2.8 grams of glycerol dimethacrylate, and Take 21 grams of Sorbitan Monooleate S-80, 57 grams of No. 200 solvent oil, a mixture of 0.154 grams of sodium persulfate and 50 grams of water, fatty alcohol polyoxyethylene ether AEO 9 Get 3.5 grams, 188 grams of water, the technological process of production is with embodiment 1.
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