Seepage-proofing thickening agent for textile printing and preparation method thereof

A textile and anti-seepage technology, which is applied in the direction of textiles, papermaking, dyeing, etc., can solve the problems of no public information and poor use effect, and achieve the effect of simple production process, low cost and easy operation control

Inactive Publication Date: 2011-02-09
LIAONING FIXED STAR FINE CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The use of this type of product has been seen in the prior art, but the use effect is not good, and there is no public information about the relevant technology

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] (1) Neutralization reaction: Add 161 grams of methacrylic acid and 55 grams of acrylic acid in a stainless steel kettle, neutralize with 332 grams of ammonia water with a concentration of 20% by weight, keep the temperature at 0-40 ° C, and adjust the pH value of the product to 6.5 , then add 18 grams of methacrylamidopropyl dimethylamine and 2.5 grams of glyceryl dimethacrylate into the reaction kettle, stir evenly to obtain neutralizing liquid;

[0018] (2) Emulsification reaction: Add 51 grams of No. 200 solvent oil to the emulsification reaction kettle, add 19 grams of sorbitan monooleate S-80, add the neutralizing solution completely while stirring at a high speed, and finally add water 170g, fully emulsified at 40-50°C for 30 minutes;

[0019] (3) Polymerization reaction: The temperature of the emulsification reaction kettle is raised to 65-68°C, and a mixture of 0.15 grams of initiator sodium persulfate and 50 grams of water is added dropwise to make it polymeriz...

Embodiment 2

[0021] The weight ratio of raw materials is: 169 grams of methacrylic acid, 59 grams of acrylic acid, 352 grams of ammonia water with a concentration of 20% by weight, 21 grams of methacrylamide propyl dimethylamine, and 3.4 grams of glycerol dimethacrylate. Take 22 grams of Sorbitan Monooleate S-80, 59 grams of No. 200 solvent oil, a mixture of 0.16 grams of sodium persulfate and 50 grams of water, fatty alcohol polyoxyethylene ether AEO 9 Get 4 grams, 198 grams of water, the technological process of production is with embodiment 1.

Embodiment 3

[0023] The weight ratio of raw materials is: 165 grams of methacrylic acid, 57 grams of acrylic acid, 342 grams of ammonia water with a concentration of 20% by weight, 20 grams of methacrylamide propyl dimethylamine, 2.8 grams of glycerol dimethacrylate, and Take 21 grams of Sorbitan Monooleate S-80, 57 grams of No. 200 solvent oil, a mixture of 0.154 grams of sodium persulfate and 50 grams of water, fatty alcohol polyoxyethylene ether AEO 9 Get 3.5 grams, 188 grams of water, the technological process of production is with embodiment 1.

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Abstract

The invention relates to a seepage-proofing thickening agent for textile printings and a preparation method thereof. The seepage-proofing thickening agent takes methacrylic acid, acrylic acid, ammonia, dimethylamine propyl methacrylamide, dimethyl acrylic acid glyceride, sorbitan monooleate S-80, 200 No. prime city naphtha, sodium persulfate and fatty alcohol polyoxyethylene ether AEO9 as raw materials and is prepared by three-step processes, i.e. neutralization, emulsification and polymerization. The seepage-proofing thickening agent contains tertiary amine groups and vinyl groups, thereby having good seepage-proofing effect and high thickening capability of a polymerisate and low viscosity coefficient and easy operation control of a reaction system.

Description

technical field [0001] The invention relates to an anti-seepage thickener for textile printing, which is used in pigment printing to obtain clear and exquisite printing patterns in pigment printing. Background technique [0002] As the textile industry enters the 21st century, it has higher requirements for the pattern fineness of printed fabrics. However, in the production process, due to the phenomenon of seepage in different links such as fabric printing, placement, and drying, the grade of the product will be reduced. An effective way to solve this kind of problem is to use an anti-seepage thickener, which is required to have high efficiency, not only has a strong thickening ability, but also has an anti-seepage function. The use of this type of product is seen in the prior art, but the use effect is not good, and there is no public information about the relevant technology. Contents of the invention [0003] The object of the present invention is to provide an anti-...

Claims

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Application Information

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Patent Type & AuthorityPatents(China)
IPC IPC(8): D06P1/52C08F220/06C08F2/24
Inventor严欣宁周明樊丽君倪成涛仇凯
OwnerLIAONING FIXED STAR FINE CHEM