Natural extract added into cigarettes, extracting method thereof and cigarettes

A technology of natural extracts and extraction methods, applied in tobacco, processed tobacco, food science, etc., can solve the problems of lack of industrial applicability, and achieve the effects of inhibiting mutagenicity, enhancing smoke, and relieving cough

Active Publication Date: 2010-02-03
SHENZHEN DABAIHUI TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the current level of my country’s harm reduction products cannot fully meet the needs of my country’s current development of Chinese-style cigarettes. There is a lack of relatively mature selective harm reduction products with high selectivity, good stability, and strong industrial applicability. Since 2005, the National Tobacco The Monopoly Bureau organized the research work on the cigarette hazard index system, and finally screened out CO, HCN, NNK, NH 3 , benzo[α]pyrene, phenol and crotonaldehyde to characterize the biohazardousness of mainstream cigarette smoke

Method used

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  • Natural extract added into cigarettes, extracting method thereof and cigarettes

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] Example 1: Grind 1 kg of dried stems and leaves of Snake dentata grape, reflux twice with 6000 ml of 95% ethanol for 2 hours and 1 hour respectively, and concentrate under reduced pressure at 0.05Mpa, 80°C, for 2 hours, until it reaches a mellow taste , add 4 times the amount of ointment and dissolve in water at a heating temperature of 80°C, filter, add 4 kg of macroporous resin column D101 to the filtrate, elute with 75% ethanol for 6 times the column volume, and recrystallize the eluate below 10°C to obtain 99% bismuth Hydromyricetin natural extract. Then, 1 gram of the natural dihydromyricetin extract containing 99% is diluted with 100 milliliters of 80% ethanol, added in 0.3% by weight of shredded tobacco, and made into cigarettes.

Embodiment 2

[0018] Example 2, crushing 1 kg of dried stems and leaves of Snake dentata grape, extracting 10 kg of 95% ethanol with 95% ethanol by percolation for 24 hours, concentrating the percolation liquid at 0.05Mpa under reduced pressure, 80°C, time 2 hours Add 4 times the amount of cream to dissolve in water until there is no alcohol smell, heat at 80°C, filter, leave the filtrate for 24 hours, crystallize, and then recrystallize below 10°C to obtain a natural extract containing 10% dihydromyricetin. Then, 1 gram of the natural dihydromyricetin extract containing 10% is diluted with 100 milliliters of 75% ethanol, added in 0.1% by weight of shredded tobacco, and made into cigarettes.

Embodiment 3

[0019] Example 3, crushing 1 kg of dried stems and leaves of Snake dentata grape, and using carbon dioxide supercritical extraction at a temperature of 35°C, a pressure of 20MPa, and a time of 2 hours to obtain coarse crystals, and then recrystallized below 10°C to obtain 50% dihydromyrica rubra Vegetarian natural extracts. Then dihydromyricetin 1 gram containing 50% dihydromyricetin natural extract is diluted with 100 milliliters of 50% ethanol, added in 0.2% by weight of shredded tobacco, and made into cigarettes.

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Abstract

The invention discloses a natural extract added into cigarettes, an extracting method thereof and cigarettes, which aim at solving the technical problem of reducing harms to the human body from the cigarettes. The natural extract can be prepared by adopting the following steps: crushing dried stem leaves of ampelopsis grossedentata, refluxing by ethanol, decompressing and concentrating at 0.05MPaand 80 DEG C for 2 hours, adding water, heating, dissolving, filtering, adding macroporous resin columns, eluting by ethanol, and recrystallizing eluant at 0-10 DEG C to obtain 99 percent of natural extract of dihydromyricetin. The cigarettes contain the natural extract of the dihydromyricetin, which accounts for 0.01-10 percent of cut tobaccos in weight percent. Compared with the prior art, the invention keeps the original taste and style of the cigarettes, can reduce the contents of nitrosamine, CO, phenol and crotonic aldehyde in cigarette smoke, and releases the adverse reactions of cough,asthma, phlegm stasis, throat obstruction, and the like caused by smoking.

Description

technical field [0001] The invention relates to an extract added to cigarettes to reduce the harm of cigarettes and an extraction method thereof, a cigarette added with the extract, especially a natural extract and its extraction method, and a cigarette added with the extract. Background technique [0002] In recent years, my country's tobacco industry has done a lot of work in the field of cigarette harm reduction technology research and application, and achieved certain results. A batch of practical additive products that reduce the harmful components of cigarette smoke have been developed and applied in cigarettes. However, the current level of my country’s harm reduction products cannot fully meet the needs of my country’s current development of Chinese-style cigarettes. There is a lack of relatively mature selective harm reduction products with high selectivity, good stability, and strong industrial applicability. Since 2005, the National Tobacco The Monopoly Bureau org...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A24B15/30A24B15/10
Inventor 温纯青温育青温玉兴
Owner SHENZHEN DABAIHUI TECH
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