A kind of maca extract and preparation method thereof
A technology of maca extract and macaene, which is applied in the field of maca extract preparation, can solve the problems that the natural active ingredients of maca have not been extracted and separated, the efficacy is not obvious, and the extraction rate is low, so as to achieve the improvement of product purity, Effect of avoiding pollution and improving extraction rate
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Embodiment 1
[0025] Select 50kg of dried Maca roots without rot, mildew, and no visible foreign impurities, and finely pulverize them until they can pass through a 60-mesh sieve; put the pulverized raw materials into the extraction tank, and add 50% alcohol solution with a weight ratio of 7 times Circulate extraction at 45°C for 2 hours to obtain the extract; put the extract into a sedimentation tank for natural precipitation for 6 hours, take the supernatant for vacuum filtration, and centrifuge the filtrate with a high-speed centrifuge at a speed of 10000r / min; take the centrifuge at 0.02~0.08 Mpa, concentrated in vacuum at 40°C to a relative density of 1.0, dried at 40°C to obtain 14kg of maca extract.
[0026] After testing, the total weight ratio of fatty acids is 30.3%, the content of benzyl isothiocyanate is 18.7%, and the total amount of macamide and macaene is 13.5%.
Embodiment 2
[0028] Select 50kg of dried Maca roots without rot, mildew, and no visible foreign impurities, and finely pulverize them until they can pass through a 100-mesh sieve; put the pulverized raw materials into the extraction tank, and add 60% alcohol solution with a weight ratio of 9 times Circulate extraction at 55°C for 5 hours to obtain the extract; put the extract into a sedimentation tank for natural precipitation for 10 hours, take the supernatant for vacuum filtration, and centrifuge the filtrate with a high-speed centrifuge at a speed of 40,000r / min; take the centrifuge at 0.02~0.08 Mpa, concentrated in vacuum at 55°C to a relative density of 1.3, dried at 55°C to obtain 12.8kg of maca extract.
[0029] After testing, the total weight ratio of fatty acids is 39.7%, the content of benzyl isothiocyanate is 26.3%, and the total amount of macamide and macaene is 20.2%.
Embodiment 3
[0031] Select 50kg of dried Maca roots without rot, mildew, and no visible foreign impurities, and finely pulverize them until they can pass through a 70-mesh sieve; put the pulverized raw materials into the extraction tank, and add 70% alcohol solution with a weight ratio of 7.5 times Circulate extraction at 50°C for 4 hours to obtain the extract; put the extract into a sedimentation tank for natural precipitation for 9 hours, take the supernatant for vacuum filtration, and centrifuge the filtrate with a high-speed centrifuge at a speed of 35000r / min; take the centrifuge at 0.02~0.08 Mpa, concentrated in vacuum at 50°C to a relative density of 1.2, dried at 45°C to obtain 12.9kg of maca extract.
[0032] After testing, the total weight ratio of fatty acids is 35.6%, the content of benzyl isothiocyanate is 24.3%, and the total amount of macamide and macaene is 18.5%.
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