Silk afterfinishing compound softening agent and preparation method

A post-finishing and softening agent technology, which is applied in the field of silk post-finishing compound softener manufacturing, can solve the problems of difficult preparation of surfactants, returns and claims for export products, high irritation and toxicity, etc., and achieve good antistatic properties, Very low yellowing, easy biodegradation effect

CN103031714AActive Publication Date: 2013-04-10ZHEJIANG HSDP SILK TECH
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Publication Date
2013-04-10
Patent Text Reader

Abstract

The invention relates to a silk afterfinishing compound softening agent and a preparation method. The softening agent is nontoxic, nonirritating, very low in yellowing possibility, good in re-wettability, biodegradable, and completely harmless to an environment. The method comprises the steps that required water temperature is selected between 0 DEG C and 100 DEG C according to used different quaternization raw materials; 1-30% of ester quaternary ammonium salt is added to water, and stirred; and then 1-30% of hydrophilic amino silicone oil is added and stirred uniformly after ester quaternary ammonium salt is completely dissolved or dispersed in the water and forms a uniform white viscous emulsion. The softening agent has the advantages that 1, the softening agent adopts raw animal or plant synthetic chemicals as main components of the softening agent, and is completely nontoxic, nonirritating, very low in yellowing possibility, and good in re-wettability, and 2, the softening agent is biodegradable and completely harmless to the environment, and is an ideal silk fabric afterfinishing softening agent.
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Description

Technical field

[0001] This application relates to a silk finishing compound softener and preparation method that is not only non-toxic, non-irritating, extremely low yellowing, and good re-wettability, but also easy to be biodegradable and completely harmless to the environment. It belongs to silk finishing compound With softener manufacturing field. Background technique

[0002] At present, the silk finishing compound softener usually uses a softener with hexadecyl octadecyl dimethyl ammonium chloride [alias: surfactant D16-1821] as the main component. This type of quaternary ammonium salt type cationic surfactant is a white or slightly yellow paste or solid. It is easily soluble in organic solvents, slightly soluble in water, and has good flexibility. It is compatible with cationic, nonionic and zwitterionic surfactants. Both have good compatibility and have always been the first choice for cosmetics, detergents and textile softeners. However, the problem is that such surfac...

Examples

Embodiment 1

[0011] Example 1: A silk finishing compound softener, the weight ratio of each component is: ester quaternary ammonium salt 1-30%, hydrophilic amino silicone oil 1-30%, water 40-100%. The quaternized raw materials in the ester quaternary ammonium salt include methyl chloride or benzyl chloride or dimethyl sulfate or diethyl sulfate. The quaternization raw materials in the ester quaternary ammonium salt are preferably dimethyl sulfate and diethyl sulfate. The best choice for the quaternization of the ester quaternary ammonium salt is dimethyl sulfate. The hydrophilic amino silicone oil is mainly formed by copolymerization of hydrogen-containing silicone oil, polyether and allyl glycidyl ether.

Embodiment 2

[0012] Example 2: On the basis of Example 1, ester quaternary ammonium salt is 1%, hydrophilic amino silicone oil is 1%, and water is 98%.

Embodiment 3

[0013] Example 3: On the basis of Example 1, ester quaternary ammonium salt is 5%, hydrophilic amino silicone oil is 5%, and water is 90%.