Positive electrode active material, preparation method, positive electrode and lithium ion secondary battery
A positive electrode active material, secondary battery technology, applied in secondary batteries, battery electrodes, chemical instruments and methods, etc., can solve the problems of difficult use of positive electrode active materials, reduced life, structural instability, etc.
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[0048] Dilute 0.03 g of antimony oxide in 50 mL of isopropanol, and then add 9 g of the Li 2 MnO 3 -LiNiCoMnO 2 , and stirred for 6 hours. Thereafter, the mixture was heated at 120° C. for 6 hours to volatilize isopropanol, and then heated at 600° C. for 6 hours to synthesize a positive electrode active material whose surface was treated with antimony. The content of transition metals in the powder was determined by inductively coupled plasma (ICP) analysis, and the characteristic peaks (003), (101), (006), (102), (102) and (104), (106), (107), (108) and (110) confirm that the crystal structure of the powder is maintained.
[0049] The thus obtained positive electrode active material, Super-P conductive agent and polyvinylidene fluoride (PVDF) binder were carried out in N-methyl-2-pyrrolidine copper (NMP) at a weight ratio of 94:3:3. Mix to form a slurry. The slurry was poured on a thin aluminum plate, and the thin aluminum plate was dried in a conventional drying oven at...
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