Degradable temporary plugging ball
A technology of temporarily blocking balls and degradable materials, which is applied in the direction of mining fluids, earthwork drilling, wellbore/well parts, etc. It can solve problems such as difficulties, non-degradation of plastic balls, and difficult steering, and achieve good mechanical strength and easy operation. Effect
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Embodiment 1
[0037] A degradable temporary blocking ball consists of the following formula (calculated by weight):
[0038] 65 parts of terephthalic acid; 75 parts of ethylene glycol; 15 parts of 1,4-butanedioic acid; 1 part of 1,3-propylene glycol; 3 parts of 1,4-benzenediol; 0.4 parts of ferric chloride; 0.2 parts of formaldehyde, 41 parts of water.
[0039] The degradable temporary blocking ball is prepared by the following steps of the following substances by weight (produced in batches of 200kg):
[0040] (1) The preparation steps of the temporary plugging ball are as attached figure 1Shown: Preparation of degradable material: ① 14 parts by weight of water, 32 parts of terephthalic acid and 38 parts of ethylene glycol, carry out esterification reaction at 250°C, add 15 parts by weight of 1 , 4-butanedioic acid, stir, obtain esterification product; Add the 1,3-propanediol that is 1 part by weight in esterification product and carry out copolymerization, control final vacuum tightnes...
Embodiment 2
[0049] A degradable temporary blocking ball consists of the following formula (calculated by weight):
[0050] 64 parts of terephthalic acid; 76 parts of ethylene glycol; 14 parts of 1,4-butanedioic acid; 2 parts of 1,3-propylene glycol; 3 parts of 1,4-benzenediol; 0.4 parts of ferric chloride; 0.2 parts of formaldehyde, 41 parts of water.
[0051] The degradable temporary blocking ball is prepared by the following steps of the following substances by weight (produced in batches of 200kg):
[0052] The preparation steps of temporary blocking ball are as attached figure 1 Shown:
[0053] 1. Preparation of degradable materials:
[0054] a. In a clean reactor, first add 14kg of clear water, heat up to 30-40°C, add 30kg of terephthalic acid and 40kg of ethylene glycol while stirring, control the addition within 30 minutes, and stir until completely dissolved after adding, Add 14 kg of 1,4-butanedioic acid, raise the temperature to 250° C., stir at a constant temperature, the...
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