Micro double-bed solid fuel decoupling combustion reaction dynamic analyzer

A kinetic analysis and combustion reaction technology, applied in the direction of chemical analysis using combustion, can solve the problems of not well reacting coke activity, changing the reaction activity of coke production, and rapid combustion process being very different, and achieving sample injection. Fast, low sample volume, simple process results
CN103543237AActive Publication Date: 2014-01-29HUAZHONG UNIV OF SCI & TECH

Patent Information

Authority / Receiving Office
CN Β· China
Patent Type
Applications(China)
Current Assignee / Owner
HUAZHONG UNIV OF SCI & TECH
Publication Date
2014-01-29

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Abstract

The invention provides a micro double-bed solid fuel decoupling combustion reaction dynamic analyzer which comprises a fuel pyrolytic reaction generation device, a residual coke combustion reaction generation device, a double-bed high-temperature coupling device, a gas path device and an analysis test device, wherein solid fuel is firstly pyrolyzed under an inert atmosphere in a micro gas flow bed; then residual cokes enter the micro gas flow bed for combustion test under an air atmosphere; a quick gas detector is used for judging a reaction mechanism by measuring a generation sequence and a generation quantity characteristic of gas components in a fuel pyrolysis process and a coke combustion process, so that reaction dynamic parameters can be calculated. According to the micro double-bed solid fuel decoupling combustion reaction dynamic analyzer, the combustion dynamic parameters of the solid fuel can be tested through direct decoupling combustion through independent and quick switching of the atmospheres and the temperature; the pyrolyzed residual cokes are directly subjected to the combustion test without a cooling process; the temperature rising rates of the gas flow bed and a fluidized bed are high, so that a combustion condition in an actual boiler can be well simulated; the measured reaction dynamic parameters are close to intrinsic reaction dynamic parameters.
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Description

technical field

[0001] The invention belongs to electric heating experimental equipment, in particular to a miniature twin-bed solid fuel decoupling combustion reaction kinetics analyzer, which is mainly applicable to the characteristics of pyrolysis reaction and coke combustion reaction of various solid fuels under decoupling combustion conditions And the test of related kinetic parameters, at the same time, it can realize the in-situ analysis test of pyrolysis residual coke. Background technique

[0002] The study of solid fuel combustion process is generally decoupled into two stages, namely, the pyrolysis of solid fuel and the combustion of coke. The pyrolysis process of solid fuel is actually that some weak bonds of the macromolecules of coal are broken when the temperature is high, so that light gaseous substances and tar are precipitated, and the remaining molecular bonds are repolymerized to form stable coal mainly composed of carbon. macromolecule. The coke left a...

Claims

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