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Infrared Spectrum Analysis and Identification Method of Cordyceps Sinensis

A technology of infrared spectrum analysis and Cordyceps sinensis, which is applied in the direction of material analysis, analysis materials, and measuring devices through optical means, can solve the problem of the indistinguishable authenticity of Cordyceps sinensis worms, and achieve rapid testing, fast analysis methods, and accurate results Effect

Active Publication Date: 2016-01-27
QINGHAI SPRING MEDICINAL RESOURCES TECHNOLOGY CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] What the present invention aims to solve is the technical problem that it is difficult to distinguish the authenticity of the Cordyceps sinensis body

Method used

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  • Infrared Spectrum Analysis and Identification Method of Cordyceps Sinensis
  • Infrared Spectrum Analysis and Identification Method of Cordyceps Sinensis
  • Infrared Spectrum Analysis and Identification Method of Cordyceps Sinensis

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0056] Example 1 The standard spectrum drawing of Cordyceps sinensis insects, the collection of essential characteristic peaks of the infrared spectrum of Cordyceps sinensis insects and the collection of common characteristic peaks of the infrared spectrum of Cordyceps sinensis insects and the determination of the lower threshold of the correlation coefficient

[0057] 1) Sample source and processing

[0058] Select 15 samples of Cordyceps sinensis from Yushu Prefecture in Qinghai, 15 from Guoluo Prefecture, 15 from Hainan Prefecture, 15 from Tibet, 15 from Sichuan, and 8 from Gansu. Samples of uniform size were selected for each origin.

[0059] The sample processing refers to the relevant regulations of the Pharmacopoeia of the People's Republic of China. The insect body part of the sample is naturally dried and crushed, and the fine powder after the 200-mesh sieve is used for the infrared spectrum test.

[0060] 2) Infrared spectroscopy instrument

[0061] In the present invention, a...

Embodiment 2

[0082] Example 2 Identification of Cordyceps Gunis and Cordyceps Sinensis

[0083] 1) Sample source and processing

[0084] The commercially available Cordyceps are numbered G1, G2, G3, G4.

[0085] The sample processing refers to the relevant regulations of the Pharmacopoeia of the People's Republic of China. The insect body part of the sample is naturally dried and crushed, and the fine powder after the 200-mesh sieve is used for the infrared spectrum test.

[0086] 2) Infrared spectroscopy instrument

[0087] All samples were tested using SpectrumOne Fourier Transform Infrared Spectrometer from PerkinElmer, USA.

[0088] Sample test parameters: Spectral scanning range 4000~400cm -1 , Spectral resolution 4cm -1 , Each spectrum is scanned 16 times cumulatively, and the interference of carbon dioxide and water vapor is deducted in real time.

[0089] 3) Infrared spectrum test method

[0090] The sample is tested using potassium bromide (KBr) tablet method. Take 1-2 mg of sample powder and...

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Abstract

The invention relates to the field of analytical chemistry, specifically to an infrared spectroscopic analysis and identification method for the polypide of Cordyceps sinensis. The objective of the invention is to overcome the technical problem that whether the polypide of Cordyceps sinensis is true or false is difficult to determine at present. Thus, the invention provides the method for rapid and accurate discrimination of the polypide of Cordyceps sinensis. The method comprises the following steps: a, drafting the standard spectrum of the polypide of Cordyceps sinensis; b, acquiring necessary infrared spectroscopic characteristic peaks and common infrared spectroscopic characteristic peaks of the polypide of Cordyceps sinensis; and c, comparing infrared spectroscopic characteristic peaks and infrared spectroscopic similarity of a detected sample of the polypide of Cordyceps sinensis. The invention provides the novel method for rapid and accurate discrimination of the polypide of Cordyceps sinensis.

Description

Technical field [0001] The invention relates to the field of analytical chemistry. Specifically, it relates to an infrared spectroscopic analysis and identification method of Cordyceps sinensis. Background technique [0002] Cordyceps sinensis is a complex of the larvae of Cordycepssinensis (Berk.) Sacc., a fungus of the ergot family, which parasitizes on the larva of the Hepialidae insect Hepialidae, and the corpse of the larva. , Deer antler is also known as the three major tonics in China. [0003] Cordyceps sinensis grows in a special environment, mainly distributed in alpine meadows and alpine shrubs at an altitude of 3000 to 5000 meters on the Qinghai-Tibet Plateau in my country. Qinghai, Tibet, Sichuan, Gansu and Yunnan are the main producing areas of Cordyceps. Qinghai ranks first in terms of output and quality of all provinces and regions. Yushu and Guoluo are the main producing areas of Cordyceps in Qinghai. Cordyceps sinensis cannot be cultivated artificially at prese...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N21/3563
Inventor 张雪峰徐丽王晓平
Owner QINGHAI SPRING MEDICINAL RESOURCES TECHNOLOGY CO LTD