Method for purifying nickel in electroless nickel plating waste liquid and nickel purifying device
A technology of electroless nickel plating and waste liquid, which is applied in the fields of optics, photographic technology, instruments, etc., can solve the problems of wrong economic and social benefits, difficult to popularize and use, and large consumption of chemicals, so as to simplify the process and reduce electric energy Consumption, no secondary environmental pollution effect
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Embodiment 1
[0028] The electroless nickel plating waste liquid is filtered, and the pH of the electroless nickel plating waste liquid is adjusted to 8 by using a sodium hydroxide solution with a mass fraction of 40-60%. Dilute sulfuric acid solution is contained in the anode box 2 . Then the electroless nickel plating waste liquid is introduced into the cathode chamber 1, so that the liquid level of the electroless nickel plating waste liquid is equal to the liquid level in the anode box 2, and the cathode 3 and the anode 4 are energized to start electrolysis. The voltage of the electrolytic process cell is 2.9V, and the current density of the waste liquid is 100A / m 2 , The temperature is 20 ~ 50 ℃. During the electrolysis process, an appropriate amount of lye is added dropwise to the anode chamber 2 to neutralize the acid produced by the electrolysis reaction, so that the pH value of the solution in the anode chamber 2 remains unchanged. During the electrolysis process, the nickel ion ...
Embodiment 2
[0030] The electroless nickel plating waste liquid is filtered, and the pH of the electroless nickel plating waste liquid is adjusted to 8 by using a sodium hydroxide solution with a mass fraction of 40-60%. Dilute sulfuric acid solution is contained in the anode box 2 . Then the electroless nickel plating waste liquid is introduced into the cathode chamber 1, so that the liquid level of the electroless nickel plating waste liquid is equal to the liquid level in the anode box 2, and the cathode 3 and the anode 4 are energized to start electrolysis. The voltage of the electrolytic process cell is 3V, and the current density of the waste liquid is 200A / m 2 , The temperature is 20 ~ 50 ℃. During the electrolysis process, an appropriate amount of lye is added dropwise to the anode chamber 2 to neutralize the acid produced by the electrolysis reaction, so that the pH value of the solution in the anode chamber 2 remains unchanged. During the electrolysis process, the nickel ion co...
Embodiment 3
[0032] The electroless nickel plating waste liquid is filtered, and the pH of the electroless nickel plating waste liquid is adjusted to 8.5 by using a sodium hydroxide solution with a mass fraction of 40-60%. Dilute sulfuric acid solution is contained in the anode box 2 . Then the electroless nickel plating waste liquid is introduced into the cathode chamber 1, so that the liquid level of the electroless nickel plating waste liquid is equal to the liquid level in the anode box 2, and the cathode 3 and the anode 4 are energized to start electrolysis. The voltage of the electrolytic process cell is 3.5V, and the current density of the waste liquid is 300A / m 2 , The temperature is 20 ~ 50 ℃. During the electrolysis process, an appropriate amount of lye is added dropwise to the anode chamber 2 to neutralize the acid produced by the electrolysis reaction, so that the pH value of the solution in the anode chamber 2 remains unchanged. During the electrolysis process, the nickel io...
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