Heat-insulating molded article and production method for same
A formed body, heat insulation technology, applied in heat exchange equipment, chemical instruments and methods, mechanical equipment, etc., can solve the problems of application field limitation, heat insulator limitation, time deterioration preparation cost, etc., to achieve excellent heat insulation performance and increased strength. Effect
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[0080] Preparation method of airgel particles
[0081] Prepare tetramethoxysilane oligomer ("methyl silicate 51", purchased from COLCOATCO., Ltd., its average molecular weight is 470) as alkoxysilane, ethanol (special grade reagent, purchased from nacalaitesqueinc.) and water As a solvent, and 0.01mol / l ammonia water as a catalyst. 1 mol of tetramethoxysilane oligomer, 120 mol of ethanol, 20 mol of water and 2.16 mol of ammonia water were mixed to prepare a sol-like reaction liquid.
[0082] Then, the sol-like reaction solution is poured into a container, and then left at room temperature to gel to produce a gelled compound.
[0083] Then, put the above-mentioned gelled compound into a place filled with liquefied carbon dioxide at a temperature of 18°C and a pressure of 5.4MPa (55kgf / cm 2 ) in a pressure vessel, and the ethanol in the gelled compound was replaced by carbon dioxide for three hours. Thereafter, the temperature and pressure of the inside of the pressure-resi...
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