A kind of TPV composition and automobile anti-collision strip material
A composition and mixture technology, applied in the field of TPV composition, can solve the problems of insufficient tensile strength and wear resistance, etc.
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[0057] The preparation method of the α, β-unsaturated carbonyl compound is:
[0058] (1) Put the weighed p-hydroxyalkylaniline in a 250mL round bottom flask, add an appropriate amount of DMF to dissolve, and cool the system to 0-5°C with an ice-water bath. While stirring, N-bromosuccinimide was added dropwise, stirred in an ice bath for 1.5-2h, then gradually returned to room temperature, and continued stirring at room temperature for 1-1.5h. After the solvent was sucked dry, it was recrystallized with chloroform and hexane to obtain 2-bromo-4-hydroxyalkylaniline. The reaction equation is as follows:
[0059]
[0060] (2) Put the weighed 2-bromo-4-hydroxyalkylaniline in a 250mL double-necked bottle, install a reflux condenser, and add an appropriate amount of toluene to dissolve. While stirring, excess aqueous formic acid was added. Then the system was heated to 110-120°C and refluxed for 4-6h. After the reaction was completed, it was cooled to room temperature, the pro...
Embodiment
[0132]
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