Method of measuring bromine in coal with high temperature hydrolysis and bromine ion selective electrode
A high-temperature hydrolysis and selective electrode technology, applied in the direction of material electrochemical variables, to achieve the effect of eliminating the memory effect of the pipeline, eliminating the matrix effect, and reducing the detection limit
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Embodiment 1
[0028] The method for the pyrohydrolysis-bromine ion selective electrode of the present embodiment to measure bromine in coal is carried out according to the following steps:
[0029] (1) Draw a standard curve:
[0030] Use an electronic balance to accurately weigh 1.19g of premium pure potassium bromide dried at 120°C for 2 hours in a beaker, add deionized water and stir thoroughly, and after fully dissolved, transfer it to a 1000ml volumetric flask and rinse with deionized water Beaker and glass rod 2-3 times, add each washing solution to the volumetric flask and make it up to the mark, shake well, and store in a plastic bottle for later use;
[0031] Take 1ml, 3ml, 5ml, 7ml, 9ml of the above-mentioned standard solution respectively, pour into five 100ml volumetric flasks rinsed with deionized water in turn and number them, then add 10ml of TISAB total ionic strength adjustment buffer solution, and finally use deionized water Dilute to 100ml and shake well for later use to ...
Embodiment 2
[0045] Under this condition, the same experimental method as above was used to test the rock standard sample GBW07406 (GSS-6) (the bromine content is 8.0±0.7μg·g -1 ), the bromine content in rock standard samples was tested many times, and the results of the bromine content in rock standard samples ranged from 7.59 to 8.24 μg·g -1 The test results are all within the error limit specified by the standard material, indicating that this method is feasible for the determination of bromine content in coal and the test results can meet the accuracy requirements.
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