Finishing agent containing bendiocarb microcapsules and application of finishing agent
A technology of microcapsule finishing and dichrocarb, applied in applications, insect nets, household appliances, etc., can solve the problems of poor anti-mosquito effect of anti-mosquito nets, achieve long-term anti-mosquito function, stable structure, and broad market foreground effect
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Embodiment 1
[0031] Embodiment 1 prepares microcapsules of evil insects by interfacial polymerization
[0032] The preparation process of the evil insect microcapsules of the present invention is as follows:
[0033] a) Preparation of the oil phase: Slightly dissolve the pest with a purity of 96.5% in dichloromethane, add TDI (toluene-2,4-diisocyanate) and mix evenly as the oil phase;
[0034] b) Prepare the water phase: use Tween 80 and Span 80 as an emulsifier with a mass ratio of 1:1, the HLB value of the emulsifier is 9.7, disperse the emulsifier in deionized water, Carry out emulsification under the speed, obtain water phase;
[0035] c) Preparation of emulsion: slowly add the oil phase of step a) to the water phase of step b) at a rotational speed of 550r / min to obtain a uniform and stable O / W emulsion;
[0036] d) Microencapsulation: transfer the emulsified emulsion into a three-necked flask, add DETA, and raise the temperature to 60°C at a stirring rate of 550r / min, and keep it w...
Embodiment 2
[0039] Embodiment 2 prepares the evil insect microcapsule by complex coacervation method
[0040] The preparation process of the compound coacervation method of the present invention is as follows:
[0041] a) Preparation of a negatively charged system: dissolving sodium tripolyphosphate in water to obtain a negatively charged solution;
[0042] b) Preparation of a positive charge system: dissolving chitosan in acetic acid, controlling the pH at 4.5, and then adding difencarb with a purity of 96.5%, to obtain a positive charge mixture;
[0043]c) Agglomeration: adding the positively charged mixed liquid in step b) dropwise to the negatively charged solution in step a), the positively charged polymer wall material and the negatively charged polymer wall material are coagulated, Control the temperature at 60°C and keep it warm for 50 minutes;
[0044] d) Microencapsulation: Add the curing agent glutaraldehyde dropwise to the coagulation product of step c), stir at a rate of 50...
Embodiment 3-5
[0047] Embodiment 3-5 contains evil bug microcapsule finishing agent
[0048] The finishing agent containing dicarbamil microcapsules includes dibafencarb microcapsules, an adhesive and a cross-linking agent, the specific composition of which is shown in Table 1.
[0049] Table 1 Composition of the finishing agent containing the micro-capsules of evil insects
[0050]
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