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Method for detecting nitrite on line through liquid core fiber resonance Raman spectrum

A technology of nitrite and liquid core fiber, which is applied in the field of Raman spectroscopy, can solve the problems of high detection limit, toxicity, and stability to be improved, and achieve the effect of simple operation and improved work efficiency

Active Publication Date: 2016-07-20
JIANGSU UNIV
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  • Abstract
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Problems solved by technology

This method requires the use of a chromogenic reagent to develop the color of the solution, and sometimes requires the consumption of reagents to treat the original water sample, and some reagents are toxic
The measuring instrument of the electrochemical sensor is simple and easy to use, but its detection limit is relatively high and its stability needs to be improved

Method used

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  • Method for detecting nitrite on line through liquid core fiber resonance Raman spectrum
  • Method for detecting nitrite on line through liquid core fiber resonance Raman spectrum
  • Method for detecting nitrite on line through liquid core fiber resonance Raman spectrum

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Embodiment Construction

[0025] The specific implementation manners of the present invention will be further described in detail below in conjunction with the accompanying drawings and embodiments. The following examples are used to illustrate the present invention, but are not intended to limit the scope of the present invention.

[0026] Such as figure 1 As shown, it is a schematic diagram of the principle of the present invention. As shown in the figure, the present invention includes three parts: a light source, an external optical path system, and an optical path receiving system. The light source adopts a laser 1 with continuously adjustable laser frequency. The external optical path system includes: a first reflector 2, a first filter 3, a first condenser lens 4, a liquid core fiber 5, a second condenser lens 6, a second filter 7, a second reflector 8, The carrier plate 15, wherein the angle of the first reflector 2 and the second reflector 8 is adjustable, the laser beam output by the laser ...

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Abstract

The invention provides a method for detecting nitrite on line through liquid core fiber resonance Raman spectrum.The method involves a light source, a reflector path system and a light path receiving processing system.A laser device with the continuously adjustable laser frequency is adopted as the light source.The reflector path system comprises a reflector, a light filter, a focusing lens and a liquid core fiber.The light path receiving processing system comprises a monochrometer, a charge coupled device, a S3C2440 chip and a touch screen.The liquid core fiber is adopted for monitoring a nitrite solution, sampling is not needed, a sample is not damaged, meanwhile, the Raman spectrum strength can be improved by 103 times through the liquid core fiber technology, the Raman spectrum strength can be improved by 106 times by adopting the resonance Raman spectrum technology, the Raman spectrum strength can be improved by 109 times by combining the liquid core fiber technology and the resonance Raman spectrum technology, the S3C2440 chip is used for processing data, a data change track is drawn on the touch screen in real time, manual operation is not needed in the whole process, and the concentration of nitrite in water can be continuously measured on line.

Description

technical field [0001] The invention relates to a method for online detection of nitrite by liquid core optical fiber resonance Raman spectroscopy, which belongs to the technical field of Raman spectroscopy. Background technique [0002] Nitrite is a highly toxic substance and a food additive. It is very similar to salt. Excessive intake of nitrite can cause poisoning and the consequences are very serious. With the rapid development of the aquaculture industry, the breeding density is increasing and the water environment is getting worse. The most prominent problem is the production of toxic substances such as nitrite. Nitrite can cause poisoning in farmed animals. The poisoning mechanism is that the ability of the blood to carry oxygen is weakened, resulting in unobvious growth of fish, abnormal color of the body surface, weakened activity, and slow response. Therefore, it is of great significance to study a fast, real-time online nitrite detection system for the aquacultu...

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/65
CPCG01N21/65
Inventor 赵德安孙海盟李道亮
Owner JIANGSU UNIV
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