Method for rapidly determining content of organic matter in soil
A technology for rapid determination of organic matter content, applied in the preparation of test samples, chemical analysis by titration, etc., can solve the problems of no unified measurement standard, uneven heating of samples, and limited use range, etc., to achieve low cost, Effect of short heating time, improved precision and readiness
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Embodiment 1
[0042] Take 12 soil samples from different locations in Guangxi, and use an elemental analyzer to measure the organic matter content of the samples in the range of 20 to 32g / kg. Take 3 samples from each sample for the test, and take the average of the results. All samples are tested in the same batch. The specific operation steps are as follows:
[0043] (1) Soil pretreatment: the soil sample is air-dried, pulverized, and passed through a 0.25mm sieve for subsequent use to obtain a soil sample;
[0044] (2) Digestion: Add 0.05g (accurate to 0.0001g) of soil sample to each digestion tube with a capacity of 100mL, and add 0.1g of bismuth nitrate, and then add 10mL of bismuth nitrate with a concentration of 0.4mol / L Potassium dichromate-concentrated sulfuric acid solution and 3mL of concentrated phosphoric acid, then place the digestion tube in the above-mentioned digestion device that has been preheated to 180°C, remove the sealing sheet, put the digestion tube into the digestio...
Embodiment 2
[0064] Six soil samples were taken from different locations in Guangxi, and the organic matter content of the samples was measured by an elemental analyzer in the range of 8-13g / kg. Three samples were taken from each sample for the test, and the results were averaged. All samples were tested in the same batch. The specific operation steps are as follows:
[0065] (1) Soil pretreatment: the soil sample is air-dried, pulverized, and passed through a 0.25mm sieve for subsequent use to obtain a soil sample;
[0066] (2) Digestion: Add 0.5g (accurate to 0.0001g) of soil sample to each digestion tube with a capacity of 100mL, add 0.3g of bismuth nitrate, and then add 15mL of bismuth nitrate with a concentration of 0.4mol / L Potassium dichromate-concentrated sulfuric acid solution and 5mL of concentrated phosphoric acid, then place the digestion tube in the above-mentioned digestion device that has been preheated to 180°C, remove the sealing sheet, and move the sealing sheet to cover ...
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