A kind of method for preparing eva elastomer
A technology of elastomer and ethylene, which is applied in the field of preparation of polymer materials, can solve the problems of high ethylene pressure, difficult control, complex process and equipment, complex solvent system, etc., achieve high industrial application value, improve diffusion and initiation efficiency, and chain transfer constant low effect
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Embodiment 1
[0027] In a single reactor, tert-butanol is used as a single solvent; the volume ratio of solvent to vinyl acetate is 2:1; the initiator is azobisisobutyronitrile, and the consumption is 3.0wt% of vinyl acetate; the polymerization temperature The temperature is 65°C, the ethylene pressure is 19.0 MPa, and the reaction time is 4 hours. Under this condition, the VAc content in the polymerization product was 49.7wt%.
Embodiment 2
[0029] In a single reactor, tert-butanol is used as a single solvent; the volume ratio of solvent to vinyl acetate is 2:1; the initiator is azobisisobutyronitrile, and the consumption is 3.0wt% of vinyl acetate; the polymerization temperature The temperature is 65°C, the ethylene pressure is 17.0 MPa, and the reaction time is 4 hours. Under this condition, the VAc content in the polymerization product was 51.1wt%.
Embodiment 3
[0031] In a single reactor, tert-butanol is used as a single solvent; the volume ratio of solvent to vinyl acetate is 2:1; the initiator is azobisisobutyronitrile, and the consumption is 3.0wt% of vinyl acetate; the polymerization temperature The temperature is 65°C, the ethylene pressure is 13.0MPa, and the reaction time is 4 hours. Under this condition, the VAc content in the polymerization product is 57.6wt%.
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