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Method for rapidly detecting content of chromium in furniture factory wastewater

A furniture factory, a technology of chromium content, applied in the measurement of color/spectral properties, material analysis by observing the effect on chemical indicators, and analysis by chemical reaction of materials, etc. The results of the measurement are inaccurate, the steps are complex, etc., to achieve high accuracy, avoid injury, and protect health.

Inactive Publication Date: 2017-04-26
郑洪均
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] The purpose of the present invention is to overcome the above-mentioned existing method for measuring chromium content in drinking water with complicated steps, and the error of the measured result is large, which is likely to cause harm to people after drinking for a long time. A method for determining the chromium content in medium, the determination process of the method is simple, and the determination result is high in accuracy, which can avoid the damage caused by excessive chromium to the human body, protect people's health, and solve the existing steps of the determination method for the chromium content in drinking water It is complicated, and the measurement results have a large error, which is likely to cause harm to people after long-term drinking

Method used

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Embodiment

[0014] A method capable of quickly realizing the determination of chromium content in furniture factory wastewater comprises the following steps:

[0015] (1) Reagent preparation: select acetone, (1+1) sulfuric acid, (1+1) phosphoric acid, 20% (m / V) urea solution, 4% (m / V) potassium permanganate solution, 2% (m / V) Sodium nitrite solution, 0.2% (m / V) sodium hydroxide solution for later use, weigh 8g of zinc sulfate, dissolve in 100mL water; weigh 2.4g of sodium hydroxide, dissolve in 120mL water, mix the above two solutions ; Weigh 0.2829g of potassium dichromate (excellent grade) dried at 120°C for 2 hours, dissolve it in water, transfer it into a 1000mL volumetric flask, dilute with water to the mark, shake well, and each ml of stock solution contains 0.100ug of hexavalent chromium; Draw 5.00mL of chromium standard stock solution into a 500mL volumetric flask, dilute with water to the marked line, shake well, each milliliter of standard use solution contains 1.00ug of hexava...

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PUM

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Abstract

The invention discloses a method for rapidly detecting the content of chromium in furniture factory wastewater. The method comprises the following steps: selecting acetone, sulfuric acid, phosphoric acid, a 20% urea solution, a 4% potassium permanganate solution, a 2% sodium nitrite solution and a 0.2% sodium hydroxide solution for later use, weighing zinc sulfate, and dissolving the zinc sulfate in water; weighing sodium hydroxide, dissolving the sodium hydroxide in water, and mixing the obtained zinc sulfate solution with the obtained sodium hydroxide solution; weighing dry potassium dichromate, dissolving the dry potassium dichromate in water, transferring the obtained solution to a 1000 mL volumetric flask, and allowing the content of hexavalent chromium in the obtained storage solution to be 0.100 [mu]g / mL; sucking 5.00 mL of the chromium standard storage solution to a 500 mL volumetric flask, and allowing the content of hexavalent chromium in the obtained standard use solution to be 1.00 [mu]g / mL; weighing 0.2 g of diphenylcarbazide, dissolving the diphenylcarbazide in 50 mL of acetone, adding water to dilute to 100 mL, reducing Cr<6+> into Cr<3+>, adjusting the pH value of a water sample to 8, adding a color developer solution, disposing the obtained water sample for 5 min, carrying out acidifying color developing, and making a standard curve by using the above same method; and calculating a result. The method has the advantages of simple detection process, high accuracy of the detection result, avoiding of damages of standard exceeding chromium to human bodies, and protection of people's health.

Description

technical field [0001] The invention relates to a method, in particular to a method capable of quickly realizing the determination of chromium content in furniture factory wastewater. Background technique [0002] Drinking water refers to water that can be directly supplied to the human body for drinking without treatment. Water is the main component of body fluid, and is an important substance that constitutes cells, tissue fluid, plasma, etc. As the medium of all chemical reactions in the body, water is a platform for the transportation of various nutrients and substances. With its 40% market share, packaged drinking water has firmly ranked the top spot in the national beverage market. In the industry, pure water, natural mineral water and mineral water manufacturers account for the largest proportion. Consumers' preferences for drinking water have changed, and the strategic focus of enterprises has also shifted to natural mineral water following the market. From Janua...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/78G01N21/31
CPCG01N21/78G01N21/31
Inventor 郑洪均
Owner 郑洪均
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