Preparation method and purpose of Chinese wolfberry extract
A technology of wolfberry extract and wolfberry, applied in the application, animal feed, animal feed and other directions, can solve the problems of environmental pollution, rough workmanship, slow absorption, etc., and achieve the effects of improving immunity, improving meat yield, and avoiding drug residues
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Embodiment 1
[0026] Embodiment 1, a preparation method of wolfberry extract, the steps are as follows:
[0027] (1) Collect the stems, leaves and fruits of Chinese wolfberry and use them as raw materials;
[0028] (2) Put the above raw materials into the alcohol ultrasonic extraction tank for one extraction, add 9 times the amount of 15% ethanol water, ultrasonic for 1.5 hours at 25°C, ultrasonic frequency 50KHz, vapor pressure 0.1MPa, and ethanol reflux;
[0029] (3) Filtration to obtain the primary filtrate and primary filter residue respectively, and the primary filtrate is passed through the reduced pressure concentration tank to recover ethanol until the recovered ethanol <60%, stop the recovery, and continue to concentrate the filtrate once to obtain a concentrate;
[0030] (4) Add 9 times the amount of 15% ethanol water to the primary filter residue for secondary extraction, ultrasonic for 1.5 hours at 25°C, ultrasonic frequency of 50KHz, vapor pressure of 0.1MPa, and ethanol reflux; the fil...
Embodiment 2
[0033] Embodiment 2, a preparation method of wolfberry extract, the steps are as follows:
[0034] (1) Collect the stems, leaves and fruits of Chinese wolfberry and use them as raw materials;
[0035] (2) Put the above raw materials into the alcohol ultrasonic extraction tank for one extraction, add 11 times the amount of 20% ethanol water, ultrasonic for 2 hours at 40°C, ultrasonic frequency 60KHz, vapor pressure 0.2MPa, ethanol reflux;
[0036] (3) Filtration to obtain the primary filtrate and primary filter residue respectively, and the primary filtrate is passed through the reduced pressure concentration tank to recover ethanol until the recovered ethanol <60%, stop the recovery, and continue to concentrate the filtrate once to obtain a concentrate;
[0037] (4) Add 11 times the amount of 20% ethanol water to the primary filter residue for secondary extraction, ultrasonic for 2 hours at 40°C, ultrasonic frequency 60KHz, vapor pressure 0.2MPa, and ethanol reflux; the filtrate is rec...
Embodiment 3
[0040] Embodiment 3, a preparation method of wolfberry extract, the steps are as follows:
[0041] (1) Collect the stems, leaves and fruits of Chinese wolfberry and use them as raw materials;
[0042] (2) Put the above raw materials into the alcohol ultrasonic extraction tank for one extraction, add 10 times the amount of 18% ethanol water, ultrasonic for 1.5 hours at 30°C, ultrasonic frequency 53KHz, vapor pressure 0.15MPa, ethanol reflux;
[0043] (3) Filtration to obtain the primary filtrate and primary filter residue respectively, and the primary filtrate is passed through the reduced pressure concentration tank to recover ethanol until the recovered ethanol <60%, stop the recovery, and continue to concentrate the filtrate once to obtain a concentrate;
[0044] (4) Add 10 times the amount of 18% ethanol water to the primary filter residue for secondary extraction, ultrasonic for 1.5 hours at 30°C, ultrasonic frequency of 53KHz, vapor pressure of 0.15MPa, and ethanol reflux; the fil...
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