Compound with anthrone as core and application thereof in organic light emission diode devices
A compound and luminescent technology, applied in the field of semiconductors, can solve problems such as performance differences, achieve the effects of improving luminous efficiency, device life, and good industrialization prospects
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Embodiment 1
[0057] Embodiment 1: the synthesis of compound 1:
[0058] synthetic route:
[0059]
[0060] In a 1L three-neck flask equipped with a constant pressure dropping funnel, add metal magnesium (0.21mol), dissolve p-bromoiodobenzene (0.20mol) in 300mL tetrahydrofuran, and place it in a constant pressure dropping funnel, using nitrogen protection , heat the three-neck flask until the temperature in the bottle reaches 65°C, add the tetrahydrofuran solution of p-bromoiodobenzene through the constant pressure dropping funnel, first add 50mL, after the reaction is triggered, slowly add the remaining part, after 1h the dropwise addition is completed, the reflux temperature Reaction at lower temperature for 2h, transferred to constant pressure funnel after cooling down to room temperature for use;
[0061] Dissolve anthraquinone (0.20mol) in 200mL tetrahydrofuran and add it to a 2L three-neck flask, then slowly add the above-mentioned solution for use dropwise, and react at reflux te...
Embodiment 2
[0066] Embodiment 2: the synthesis of compound 3:
[0067] synthetic route:
[0068]
[0069] In a 1L three-neck flask equipped with a constant pressure dropping funnel, add metal magnesium (0.21mol), dissolve bromobenzene (0.20mol) in 300mL tetrahydrofuran, and place in the constant pressure dropping funnel, use nitrogen protection, heat When the temperature in the three-necked flask reaches 65°C, add the tetrahydrofuran solution of bromobenzene through a constant-pressure dropping funnel, first add 50 mL, and after the reaction is triggered, slowly add the remaining part dropwise, after 1 hour of dropwise addition, react at reflux temperature for 2 hours. After cooling down to room temperature, it was transferred to a constant pressure funnel for use;
[0070] Dissolve 2-bromoanthraquinone (0.080mol) in 200mL tetrahydrofuran and add it to a 2L three-neck flask, then slowly add the above-mentioned solution for use dropwise, and react at reflux temperature for 3h. The sol...
Embodiment 3
[0074] Embodiment 3: the synthesis of compound 6:
[0075] synthetic route:
[0076]
[0077] In a 1L three-neck flask equipped with a constant pressure dropping funnel, add metal magnesium (0.21mol), dissolve p-bromoiodobenzene (0.20mol) in 300mL tetrahydrofuran, and place it in a constant pressure dropping funnel, using nitrogen protection , heat the three-neck flask until the temperature in the bottle reaches 65°C, add the tetrahydrofuran solution of p-bromoiodobenzene through the constant pressure dropping funnel, first add 50mL, after the reaction is triggered, slowly add the remaining part, after 1h the dropwise addition is completed, the reflux temperature Reaction at lower temperature for 2h, transferred to constant pressure funnel after cooling down to room temperature for use;
[0078] Dissolve anthraquinone (0.08mol) in 200mL tetrahydrofuran and add it to a 2L three-necked flask, then slowly add the above-mentioned solution for use dropwise, and react at reflux ...
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