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Masking liquid for dental zirconium oxide ceramic as well as preparation method and application thereof

A zirconia ceramic and zirconia technology, applied in the field of dental ceramics, can solve the problems of inability to present natural simulation, large color difference between adjacent teeth, complex composition of raw materials, etc., to improve internal transparency, low production cost, and preparation method. Simple to use effect

Pending Publication Date: 2018-12-28
AIDITE (QINHUANGDAO) TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] However, it is found that zirconia ceramics, as the most rational dental restoration material, still have significant defects in practical applications: First, if the abutment is dark in color or a metal abutment is planted during use, the zirconia all-ceramic crown will show through. The color of the abutment teeth or the black color of the metal abutment will cause a large difference in color with the adjacent teeth, and the effect of natural simulation cannot be presented; secondly, the method of dyeing dental zirconia ceramics in the prior art is complicated and the raw materials Complex composition and high cost of raw materials

Method used

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  • Masking liquid for dental zirconium oxide ceramic as well as preparation method and application thereof

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Embodiment 1

[0029] Embodiment 1 of the present invention discloses a color-masking liquid for dental zirconia ceramics, its preparation method and application.

[0030] A kind of opacifying liquid for dental zirconia ceramics, comprising Al(NO 3 ) 3 "9H 2 O 1.0g, methyl orange indicator 0.08g, PEG400 10g and deionized water 100g.

[0031] A preparation method for dental zirconia ceramics opaquer, specifically comprising the following steps:

[0032] (1) Weigh 1.0gAl(NO 3 ) 3 "9H 2 0, 0.08g methyl orange and 10g PEG400, and measure 100g deionized water for subsequent use;

[0033] (2) Al(NO 3 ) 3 "9H 2 O was added to deionized water, and then the overall mixed system was added to an ultrasonic cleaner, and the ultrasonic vibration power was set to 300W. After 30 minutes of ultrasonic vibration and mixing, until the opacifying agent was completely dissolved to obtain a 0.027mol / L mixed solution;

[0034] (3) Next, add methyl orange and PEG400 to the above mixed solution, continue ...

Embodiment 2

[0039] Embodiment 2 of the present invention discloses a color-masking liquid for dental zirconia ceramics and its preparation method and application.

[0040] A kind of opacifying liquid for dental zirconia ceramics, comprising Al(NO 3 ) 3 "9H 2 O 20g, tartrazine indicator 0.12g, PEG400 15g and deionized water 100g.

[0041]A preparation method for dental zirconia ceramics opaquer, specifically comprising the following steps:

[0042] (1) Weigh 20g Al(NO 3 ) 3 "9H 2 0, 0.12g tartrazine and 15g PEG400, and measure 100g deionized water for subsequent use;

[0043] (2) Al(NO 3 ) 3 "9H 2 O was added to deionized water, and then the overall mixed system was added to an ultrasonic cleaner, and the ultrasonic vibration power was set to 200W. After 50 minutes of ultrasonic vibration and mixing, until the opacifying agent was completely dissolved to obtain a 0.53mol / L mixed solution;

[0044] (3) Then add tartrazine and PEG400 to the above mixed solution, continue to set the...

Embodiment 3

[0049] Embodiment 3 of the present invention discloses a color-masking liquid for dental zirconia ceramics and its preparation method and application.

[0050] A kind of opacifying liquid for dental zirconia ceramics, comprising Al(NO 3 ) 3 "9H 2 O 50g, methyl orange indicator 0.1g, anthocyanin indicator 0.1g, PEG400 20g and deionized water 100g.

[0051] A preparation method for dental zirconia ceramics opaquer, specifically comprising the following steps:

[0052] (1) Weigh 50g Al(NO 3 ) 3 "9H 2 O, 0.1g methyl orange, 0.1g anthocyanins and 20g PEG400, and measure 100g deionized water for subsequent use;

[0053] (2) Al(NO 3 ) 3 "9H 2 O was added to deionized water, and then the overall mixed system was added to an ultrasonic cleaner, and the ultrasonic vibration power was set to 100W. After 45 minutes of ultrasonic vibration and mixing, until the opacifying agent was completely dissolved to obtain a 1.33mol / L mixed solution;

[0054] (3) Then add methyl orange, ant...

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Abstract

The invention discloses a masking liquid for a dental zirconium oxide ceramic. The masking liquid comprises a masking agent, a color indicating agent, an additive and deionized water. The masking liquid can reduce the transparency in a tooth restoration without affecting the color effect out of the restoration. Meanwhile, the invention also discloses a preparation method of the masking liquid forthe dental zirconium oxide ceramic. The preparation method has the obvious advantages of simple process, low manufacturing cost and good repeatability. Moreover, the invention also discloses application and an application method of the masking liquid for the dental zirconium oxide ceramic. The problem that the transparency in the dental zirconium oxide ceramic is too high can be improved obviously, so that the finally obtained tooth restoration can obtain a natural emulational effect.

Description

technical field [0001] The invention relates to the technical field of dental ceramics, in particular to a color-masking liquid for dental zirconia ceramics and a preparation method and application thereof. Background technique [0002] At present, dental ceramics refer to glass ceramic materials and products used for dental treatment and restoration, which belong to the category of medical devices. Zirconia ceramics have excellent mechanical properties, its bending strength exceeds 1000MPa, and a relatively thin thickness can achieve high strength, so it is an ideal dental restoration material. In dental restorative treatment, the restoration should not only have certain strength, wear resistance, corrosion resistance and biocompatibility, but also have good aesthetic properties. Especially in recent years, with the improvement of national living standards, patients have higher and higher requirements for the similarity between dental restorations and natural teeth in appe...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B41/85
CPCC04B41/009C04B41/50C04B41/5009C04B41/85C04B35/48C04B41/0072
Inventor 李洪文王秀梅周生刚吴海艳谢银霞
Owner AIDITE (QINHUANGDAO) TECH CO LTD
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