The invention relates to a preparation method for a
spirogyra-based
biomass carbon material / nanometer
sulfur composite material. The method comprises the following steps of washing and
drying spirogyra, heating the washed and dried
spirogyra in a vacuum tubular furnace, carrying out heat preservation and
carbonization at 500-900 DEG C, mixing the carbonized spirogyra with nanometer
sulfur with
ultrasound, carrying out ball milling,
drying the ball-milled mixture by an air blow
drying box, heating the dried mixture in the vacuum tubular furnace, carrying out heat preservation for 3-6 hours at 100-200 DEG C, and afterwards cooling the mixture subjected to heat preservation to a
room temperature with the furnace to obtain the target product, namely the spirogyra-based
biomass carbon / nanometer
sulfur composite material. According to the preparation method, the spirogyra is taken as a precursor for the first time, and a
biomass carbon material with a continuous sheet-shaped structure similar to
graphene and with nanoscale thickness is synthesized; the
biomass carbon material comprises the sheet-shaped structure composed of continuous fibers, also is provided with nanoscale pores and is high in uniformity and continuity, the loading of sulfur particles is facilitated, and the obtained
composite material has favorably electrochemical performance.