Colority and turbidity compensation determination method for ammonia nitrogen in distilled spirit industrial wastewater
A technology of industrial wastewater and measurement methods, which is applied in the direction of color/spectral characteristic measurement, measurement devices, and material analysis through optical means. It can solve the problems of long measurement time and low work efficiency, and overcome the influence of detection results. The effect of work efficiency
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[0028] 1 Reagents and materials
[0029] 1.1 Potassium sodium tartrate solution, ρ=500g / L.
[0030] Weigh 50.0g potassium sodium tartrate (KNaC 4 h 6 o 6 4H 2 O) Dissolve in 100mL of water, heat to boil to drive off ammonia, fully cool and dilute to 100mL.
[0031] 1.2 Nessler's reagent solution
[0032] Weigh 16.0g of sodium hydroxide (NaOH), dissolve it in 50mL of water, and cool to room temperature. Weigh 7.0g potassium iodide (KI) and 10.0g mercury iodide (HgI 2 ), dissolved in water, and then this solution was slowly added to the above 50mL sodium hydroxide solution under stirring, and diluted with water to 100mL. Store in polyethylene bottles, tightly closed with rubber stoppers or polyethylene caps, and stored in a dark place, valid for one year.
[0033] 1.3 Chromaticity-Turbidity Compensation Solution
[0034] Mix one volume of sodium hydroxide solution (160 g / L) and one volume of potassium sodium tartrate solution (1.1).
[0035] 1.4 Ammonia nitrogen standa...
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