Method for extracting and preparing arthritisChinese patent medicine from ginger
A technology for arthritis and Chinese patent medicines, which is applied in the field of extracting and preparing Chinese patent medicines for arthritis diseases from ginger, which can solve the problems that extracts are difficult to prepare, and raw materials, extracts and finished preparations are not proposed or formulated.
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Embodiment 1
[0018] Embodiment 1: The effective fraction volatile oil and 6-Gingerol of ginger are prepared by pressing method
[0019] Take ginger, remove impurities, and press with a press for 3 hours to obtain crude ginger oil, wherein the content of volatile components is 67%, and the content of 6-Gingerol is 0.1-5%.
Embodiment 2
[0020] Embodiment 2: adopt solvent method to prepare the effective part of ginger
[0021] (1) cold immerse twice with petroleum ether or gasoline, each time for 24 hours, add 6 times the amount of solvent each time, get crude oil, filter, get ginger oil, wherein the content is 92% if the volatile component is the effective part , with 6-Gingerol as the active ingredient content up to 1.2%.
[0022] (2) Petroleum ether or gasoline reflux extraction 3 times, 2 hours each time, add 4 times the amount of solvent each time, to obtain crude oil, filter, to obtain ginger extract, wherein the content is 80% if the volatile components are the effective parts , with 6-Gingerol as the active ingredient content up to 2.0%.
Embodiment 3
[0023] Embodiment 3: adopt supercritical carbon dioxide extraction method to prepare the volatile component of ginger and 6-Gingerol
[0024] Using supercritical carbon dioxide extraction method, extract twice, the first time pressure 35Mpa, temperature 30°C, time 2 hours, the second time pressure 40Mpa, temperature 40°C, time 3 hours, to get crude oil, filter to get ginger extract , wherein the content is 89% when the volatile component is the effective part, and the content reaches 4.6% when the active component is 6-Gingerol.
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