A device and process for producing aromatic products

An aromatic hydrocarbon and isomerization technology, which is applied in the purification/separation of hydrocarbons, isomerization to hydrocarbon production, and organic chemistry, etc. It can solve the problem of increasing the fuel consumption of the xylene reboiler, increasing the operating load and cooling load of the xylene tower. It can reduce the degree of back mixing, improve the thermodynamic efficiency, and reduce the condensation load.

Active Publication Date: 2022-03-08
CHINA PETROLEUM & CHEM CORP +1
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In this process, the rectification of the extracted liquid is a double-tower process of the extracted liquid tower and the finished product tower, which consumes a lot of energy, and after the isomerization product is removed by the deheptanizer to remove light hydrocarbons below C7, Most of it is recycled back to the xylene tower, increasing the operating load of the xylene tower and increasing the fuel consumption of the xylene reboiler
In addition, all isomerized products must be cooled. After the hydrogen gas that has not participated in the reaction is separated, the cooling load is relatively large; the material after the hydrogen gas is separated needs to be reheated, and it enters the deheptanizer for further separation. The material is cooled first and then heated. problem, resulting in a waste of energy

Method used

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  • A device and process for producing aromatic products
  • A device and process for producing aromatic products
  • A device and process for producing aromatic products

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Effect test

Embodiment 1

[0065] Embodiment 1 illustrates the method and energy consumption of the novel p-xylene production process provided by the present invention, wherein the isomerization reaction rectification overhead product directly leaves the device without separation, and the hydrogen required for the isomerization reaction is boosted by a compressor Afterwards, it is mixed with the isomerization reaction feed. The energy consumption of the device is shown in Table 2.

[0066] Table 1

[0067]

[0068] Table 2

[0069]

[0070] As can be seen from Table 1 and Table 2, compared with Comparative Example 1, the method for producing p-xylene provided by the invention can save a set of rectification tower, cooler reboiler equipment and a gas-liquid separation tank, air cooling equipment, water coolers and a separate isomerization reactor. Adopting the method provided by the invention not only reduces the number of equipment, but also reduces energy consumption by 19.8%. Therefore, adop...

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Abstract

The invention discloses a device and a process for producing aromatic products. A device for producing aromatic products in the present invention comprises a xylene fractionation unit, an adsorption separation unit and an isomerization reaction unit; the adsorption separation unit comprises an adsorption separation tower, an extraction liquid fractionation tower, a raffinate tower and a heat exchange unit Device II; the isomerization reaction unit includes an isomerization reaction rectification tower, a clay tower, an isomerization reaction heating furnace, a heat exchanger III, a heat exchanger IV, a heat exchanger VI and a compressor. The invention also provides a process for producing aromatic products. The invention reduces the equipment investment, reduces the operating load of the xylene tower, saves the fuel gas consumption of the xylene reboiler, and simultaneously performs the isomerization reaction and the product separation to realize the coupled utilization of energy; optimize the heat exchange The network reduces the fuel gas consumption of the isomerization reaction heating furnace, greatly reduces energy consumption, and improves economic and social benefits.

Description

technical field [0001] The invention relates to a device and process for producing aromatic products. Background technique [0002] P-xylene is one of the important basic organic raw materials in the petrochemical industry. It is mainly used to produce terephthalic acid (PTA) and dimethyl terephthalate (DMT). It is widely used in chemical fibers, synthetic resins, pesticides, and medicines. , plastics and other production areas. In 2017, the apparent consumption of p-xylene in my country will reach 2400×10 4 t, the production capacity of p-xylene unit reaches 816×10 4 t, accounting for about 20% of global production capacity, my country is already the world's largest producer of p-xylene. [0003] C 8 Aromatics include o-xylene, p-xylene, m-xylene and ethylbenzene four isomers, among which p-xylene has the largest market, so the industry usually prefers to increase the specific C 8 The production of para-xylene from aromatics feedstock sources even maximizes it. Due to...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C07C5/27C07C7/00C07C7/04C07C7/13C07C15/08
CPCC07C7/005C07C7/13C07C7/04C07C5/2732C07C15/08
Inventor 胡珺张英高明薄德臣
Owner CHINA PETROLEUM & CHEM CORP
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